N-(苯基亚甲基)-环己胺合成路线 （共 53 条）
反应条件
Rh(I)Cl(CO)(PMe3)2
16.5 h; Ambient temperatureIrradiation; Yield given. Yields of byproduct given;
参考文献
Tanaka, Masato; Sakakura, Toshiyasu; Tokunaga, Yuko; Sodeyama, Touru
Chemistry Letters, 1987 , p. 2373 - 2374
反应条件
in chloroform
0.666667 h; Ambient temperatureother primary and secondary amines; var. temp., times and solvents; Product distribution;
参考文献
Vidal, Joelle; Drouin, Jacques; Collet, Andre
Journal of the Chemical Society, Chemical Communications, 1991 , # 6 p. 435 - 437
参考文献
Shono,T. et al.
Bulletin of the Chemical Society of Japan, 1964 , vol. 37, p. 635 - 637
参考文献
Jarvis, Bruce B.; Nicholas, Paul, E.
Journal of Organic Chemistry, 1980 , vol. 45, # 11 p. 2265 - 2268
反应条件
1: 59 percent / tetrahydrofuran / 312 h / Ambient temperature
2: 1.) LDA / 1.) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, RT, 20 h
3: 4 percent / AlCl3 / CH2Cl2 / 24 h / Ambient temperature
View Scheme
参考文献
Iwama, Tetsuo; Takagi, Atsuko; Kataoka, Tadashi
Chemical and Pharmaceutical Bulletin, 1998 , vol. 46, # 5 p. 757 - 766
反应条件
in acetic acid
T=25°C; 0.25 h;
参考文献
Singh, Serjinder; Singh, Iqbal
Journal of the Chemical Society, Chemical Communications, 1982 , # 17 p. 1000 - 1001
反应条件
in acetic acid
T=25°C; 0.25 h;
参考文献
Singh, Serjinder; Singh, Iqbal
Journal of the Chemical Society, Chemical Communications, 1982 , # 17 p. 1000 - 1001
反应条件
in neat (no solvent)
T=130 - 135°C; 0.166667 h;
参考文献
Masayuki, Sato; Ogasawara, Hiromichi; Yoshizumi, Eriko; Kato, Tetsuzo
Chemical & Pharmaceutical Bulletin, 1983 , vol. 31, # 6 p. 1902 - 1909
反应条件
dicobalt octacarbonyl; carbon monoxide; hydrogen; benzene
T=135°C; P=132391 Torr;
参考文献
Nakamura; Hagihara
Memoirs of the Institute of Scientific and Industrial Research, Osaka University, 1958 , vol. 15, p. 195,196
反应条件
LaNi5 hydride in tetrahydrofuran; methanol
1) 0 deg C, 6 h, 2) r.t., 13 h;
参考文献
Imamoto, Tsuneo; Mita, Takeshi; Yokoyama, Masataka
Journal of the Chemical Society, Chemical Communications, 1984 , # 3 p. 163 - 164
