5,10,15,20-四三(4-甲氧基苯基)-21H,23H-卟啉合成路线 (共 34 条)
反应条件
1: With Tulsion-63 resin; 1,1,1-triethoxyethane in dichloromethane T=20°C; 17 h; 2: With chloranil in dichloromethane 2 h; Heating;
参考文献
Naik, Rajan; Joshi, Padmakar; Kaiwar, Sharada P.; Deshpande, Rajesh K.
Tetrahedron, 2003 , vol. 59, # 13 p. 2207 - 2213
反应条件
1: CF3SO2Cl / CH2Cl2 / 1 h / 20 °C 2: air / CH2Cl2 / 3 h / 39 °C View Scheme
参考文献
Tetrahedron, , vol. 60, # 8 p. 1863 - 1868
反应条件
1: With Indion-130 resin in dichloromethane T=25°C; 17 h; 2: With chloranil in dichloromethane 3 h; Heating;
参考文献
Naik, Rajan; Joshi, Padmakar; Kaiwar, Sharada P.; Deshpande, Rajesh K.
Tetrahedron, 2003 , vol. 59, # 13 p. 2207 - 2213
反应条件
18-crown-6 ether; potassium carbonate in tetrahydrofuran 24 h; Heating;
参考文献
Andou, Yoshito; Ishikawa, Kazuki; Shima, Kensuke; Shiragami, Tsutomu; Yasuda, Masahide; Inoue, Haruo
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 8 p. 1757 - 1760
反应条件
18-crown-6 ether; potassium carbonate in acetonitrile 24 h; Heating;
参考文献
Andou, Yoshito; Ishikawa, Kazuki; Shima, Kensuke; Shiragami, Tsutomu; Yasuda, Masahide; Inoue, Haruo
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 8 p. 1757 - 1760
反应条件
1: With trifluoroacetic acid in dichloromethane T=20°C; 2 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=20°C; 2 h;
参考文献
Journal of Medicinal Chemistry, , vol. 49, # 11 p. 3293 - 3304
反应条件
18-crown-6 ether; potassium carbonate in acetonitrile 24 h; Heating;
参考文献
Andou, Yoshito; Ishikawa, Kazuki; Shima, Kensuke; Shiragami, Tsutomu; Yasuda, Masahide; Inoue, Haruo
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 8 p. 1757 - 1760
反应条件
1: With boron trifluoride diethyl etherate in chloroform 1 h; DarknessInert atmosphere; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform 1 h;
参考文献
Organic Letters, , vol. 12, # 5 p. 1036 - 1039
反应条件
18-crown-6 ether; potassium carbonate in acetonitrile 24 h; Heating;
参考文献
Andou, Yoshito; Ishikawa, Kazuki; Shima, Kensuke; Shiragami, Tsutomu; Yasuda, Masahide; Inoue, Haruo
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 8 p. 1757 - 1760
反应条件
1: With ethanol; compound with boron fluoride in dichloromethane T=20°C; 1 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane
参考文献
Geier III, G. Richard; Lindsey, Jonathan S.
Tetrahedron, 2004 , vol. 60, # 50 p. 11435 - 11444