5,10,15,20-四三(4-甲氧基苯基)-21H,23H-卟啉合成路线 (共 34 条)
反应条件
chloranil in tetrahydrofuran; water Yield given;
参考文献
Journal of Organic Chemistry, , vol. 61, # 11 p. 3623 - 3634
反应条件
air; nitrobenzene; triethylamine in acetic acid T=120°C; 1 h; Yield given. Yields of byproduct given;
参考文献
Heterocycles, , vol. 43, # 7 p. 1423 - 1437
反应条件
1: With methanesulfonic acid in dichloromethane 0.5 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane 0.166667 h;
参考文献
Shaw, Janet L.; Garrison, Shana A.; Aleman, Elvin A.; Ziegler, Christopher J.; Modarelli, David A.
Journal of Organic Chemistry, 2004 , vol. 69, # 22 p. 7423 - 7427
反应条件
18-crown-6 ether; potassium carbonate in acetonitrile 24 h; Heating;
参考文献
Andou, Yoshito; Ishikawa, Kazuki; Shima, Kensuke; Shiragami, Tsutomu; Yasuda, Masahide; Inoue, Haruo
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 8 p. 1757 - 1760
反应条件
1: With trifluoroacetic acid in dichloromethane T=20°C; 0.5 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane 1 h; Heating; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 46, # 35 p. 5935 - 5939
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane 3 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane
参考文献
Stute, Silvio; Gloe, Kerstin; Gloe, Karsten
Tetrahedron, 2005 , vol. 61, # 11 p. 2907 - 2912
反应条件
potassium carbonate in N,N-dimethyl-formamide 2 h; Heating; Yield given;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 54, # 7 p. 1599 - 1603,1423 - 1426
反应条件
in propionic acid 1 h; Heating;
参考文献
Schneider, Hans-Joerg; Wang, Manxue
Journal of Organic Chemistry, 1994 , vol. 59, # 24 p. 7473 - 7478
反应条件
nitrobenzene in acetic acid Condensation; cyclization, oxidation, Rothenmund reaction; 1 h; Heating;
参考文献
Photochemistry and Photobiology, , vol. 72, # 2 p. 217 - 225
反应条件
propionic acid Heating;
参考文献
Organic Letters, , vol. 8, # 12 p. 2595 - 2598