5,10,15,20-四(4-氨基苯基)卟啉合成路线 （共 11 条）
反应条件
hydrogenchloride; tin(ll) chloride T=80°C; 0.5 h;
参考文献
Semeikin, A. S.; Koifman, O. I.; Berezin, B. D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1982 , vol. 18, # 10 p. 1046 - 1047
Khimiya Geterotsiklicheskikh Soedinenii, 1982 , vol. 18, # 10 p. 1354 - 1355
反应条件
pyridine; pyridine hydrochloride 2 h; Inert atmosphere;
参考文献
UNIVERSITAeT ZUeRICH; LUEDTKE, Nathan; ALZEER, Jawad; VUMMIDI, Balayeshwanth R.
Patent: WO2010/28780 A2, 2010 ;
Location in patent: Page/Page column 25 ;
反应条件
1.1: Ac2O / propionic acid / 0.5 h / Heating 1.2: 14 percent / pyridine / 1 h / Heating 2.1: 92 percent / SnCl2*H2O / aq. HCl / 0.5 h / 70 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 126, # 36 p. 11128 - 11129
反应条件
hydrogenchloride; tin(ll) chloride T=75°C; 24 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of the American Chemical Society, , vol. 114, # 17 p. 6928 - 6930
反应条件
1: With acetic anhydride in acetic acid 2: With hydrogenchloride; tin(ll) chloride
参考文献
Molecules, , vol. 5, # 12 p. 1265 - 1280
反应条件
1: nitric acid / chloroform / 0.83 h / 0 °C / Inert atmosphere 2: hydrogenchloride; tin(ll) chloride / water View Scheme
参考文献
Tetrahedron, , vol. 67, # 33 p. 6030 - 6035
反应条件
1: 5,10,15,20-tetrakis(4-carboxyphenyl)porphyrin With hydroxylamine hydrochloride T=100 - 160°C; 3 h; 2: methanol With sulfuric acid T=20°C; 36 h; Reflux;
参考文献
Journal of Organic Chemistry, , vol. 78, # 12 p. 6040 - 6049
反应条件
hydrogenchloride; sodium hydroxide; tin(ll) chloride 1.) from 75 to 80 deg C, 24 h, 2.) 1 h; Yield given. Multistep reaction. Further byproducts given. Yields of byproduct given;
参考文献
Journal of the Chinese Chemical Society, , vol. 44, # 1 p. 23 - 31
反应条件
hydrogenchloride; sodium nitrite 1.)5 deg C 2.)heating; Yield given. Multistep reaction;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , p. 1082 - 1084
Khimiya Geterotsiklicheskikh Soedinenii, , vol. 19, # 10 p. 1359 - 1361
反应条件
tetrafluoroboric acid; copper; sodium nitrite
1)H2O,5 deg C, 2) 100 deg C; Yield given. Multistep reaction;
参考文献
Semeikin, A.S.; Koifman, O.I.; Berezin, B.D.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1986 , vol. 22, # 4 p. 397 - 401
Khimiya Geterotsiklicheskikh Soedinenii, 1986 , vol. 22, # 4 p. 486 - 490
