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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-氯苯基缩水甘油醚
合成路线
（共 38 条）
2212-05-7
4-氯苯基缩水甘油醚
→
反应条件
112652-61-6
反应条件
water; chiral Co(III) salen-based in tetrahydrofuran Title compound not separated from byproducts;
参考文献
Bredikhin; Strunskaya; Novikova; Azancheev; Sharafutdinova; Bredikhina
Russian Chemical Bulletin, 2004 , vol. 53, # 1 p. 213 - 218
2212-05-7
4-氯苯基缩水甘油醚
→
反应条件
112652-61-6
反应条件
chiral salen-based cobalt(III); water in dichloromethane T=0 - 20°C; Jacobsen's hydrolytic kinetic resolution;
参考文献
Tetrahedron Asymmetry, , vol. 13, # 21 p. 2303 - 2310
2212-05-7
4-氯苯基缩水甘油醚
→
反应条件
反应条件
trimethylsilylazide; isopropylamine; β-cyclodextrin in ethanol; water T=37°C; racemat resolution; 5 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 10, # 22 p. 4261 - 4264
2212-05-7
4-氯苯基缩水甘油醚
+
4248-19-5
氨基甲酸叔丁酯
→
反应条件
1173884-50-8
反应条件
Jacobsen's (R,R)-(salen)Co(III) catalyst; 1-n-butyl-3-methylimidazolium hexafluorophosphate; 4-nitro-benzoic acid T=20°C; 7.5 h; optical yield given as percent eeenantioselective reaction;
参考文献
European Journal of Organic Chemistry, , # 17 p. 2863 - 2871
2212-05-7
4-氯苯基缩水甘油醚
+
621-84-1
氨基甲酸苄酯
→
反应条件
1173884-60-0
反应条件
Jacobsen's (R,R)-(salen)Co(III) catalyst; 1-n-butyl-3-methylimidazolium hexafluorophosphate; 4-nitro-benzoic acid T=20°C; 7.5 h; optical yield given as percent eeenantioselective reaction;
参考文献
European Journal of Organic Chemistry, , # 17 p. 2863 - 2871
2212-05-7
4-氯苯基缩水甘油醚
+
51-79-6
氨基甲酸乙酯
→
反应条件
1173884-59-7
反应条件
Jacobsen's (R,R)-(salen)Co(III) catalyst; 1-n-butyl-3-methylimidazolium hexafluorophosphate; 4-nitro-benzoic acid T=20°C; 6 h; optical yield given as percent eeenantioselective reaction;
参考文献
European Journal of Organic Chemistry, , # 17 p. 2863 - 2871
2212-05-7
4-氯苯基缩水甘油醚
→
反应条件
104-29-0
氯苯甘醚
反应条件
Bacillus megaterium ECU1001 epoxide hydrolase in potassium phosphate buffer; dimethyl sulfoxide T=30°C; pH=7; 0.5 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 9 p. 1510 - 1518
2212-05-7
4-氯苯基缩水甘油醚
→
反应条件
112652-61-6
反应条件
water; chiral Co(III) salen-based in tetrahydrofuran Title compound not separated from byproducts;
参考文献
Russian Chemical Bulletin, , vol. 53, # 1 p. 213 - 218
2212-05-7
4-氯苯基缩水甘油醚
→
反应条件
104-29-0
氯苯甘醚
反应条件
β-cyclodextrin in methanol; water T=40°C; 10 h;
参考文献
Reddy, M. Anjun; Reddy, L. Rajender; Bhanumathi, N.; Rao, K. Rama
Organic Preparations and Procedures International, 2002 , vol. 34, # 5 p. 537 - 540
2212-05-7
4-氯苯基缩水甘油醚
+
139-02-6
苯酚钠
→
反应条件
104-29-0
氯苯甘醚
+
112718-82-8
反应条件
β-cyclodextrin in water T=60°C; 8 h;
参考文献
Journal of Organic Chemistry, , vol. 76, # 6 p. 1883 - 1886
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