3,4,5,6-四氢-2H-氮杂卓合成路线 (共 6 条)
反应条件
1: With tert-butylhypochlorite in diethyl ether T=20°C; 0.5 h; 2: With sodium methylate in methanol; diethyl ether T=20°C;
参考文献
Bock, Hans; Dammel, Ralph
Chemische Berichte, 1987 , vol. 120, p. 1971 - 1986
反应条件
potassium tert-butylate T=76.9 - 96.9°C; P=0.008 - 0.08 Torr; Yield given;
参考文献
Bock, Hans; Dammel, Ralph
Chemische Berichte, 1987 , vol. 120, p. 1971 - 1986
反应条件
enzyme-substance from peas-seedlings
参考文献
Cragg, John E.; Herbert, Richard B.; Kgaphola, Mashupye M.
Tetrahedron Letters, 1990 , vol. 31, # 47 p. 6907 - 6910
反应条件
tri-ruthenium(0)dodecacarbonyl; N-phenyl-2-(dicyclohexylphosphino)pyrrol in cyclohexane T=140°C; 21 h; Inert atmosphereSchlenk techniqueAutoclave; Reagent/catalyst;
参考文献
Pingen, Dennis; Vogt, Dieter
Catalysis Science and Technology, 2014 , vol. 4, # 1 p. 47 - 52
反应条件
oxygen; copper(l) chloride T=100°C; 19 h; neat liquid; chemoselective reaction;
参考文献
Patil, Rajendra D.; Adimurthy, Subbarayappa
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 10 p. 1695 - 1700
反应条件
hydrogen; magnesium oxide; nickel T=109.85°C; Product distribution; Further Variations:CatalystsTemperatures;
参考文献
Salagre; Medina; Serra; Sueiras; Cesteros
Journal of Catalysis, 2002 , vol. 209, # 1 p. 202 - 209