二(苯基)砷烷基氧基-二(苯基)砷合成路线 （共 43 条）
反应条件
1: tetrahydrofuran / 2 h / Heating
2: H2O / tetrahydrofuran / Heating
View Scheme
参考文献
Ellermann, Jochen; Lietz, Martin
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1980 , vol. 35, # 12 p. 1514 - 1517
反应条件
1: LDA / tetrahydrofuran / 0.5 h / -40 °C
2: 81 percent / tetrahydrofuran / 1) -40 deg C, 2) 30 min, reflux
3: 100 percent / LiAlH4 / tetrahydrofuran / 0 °C
4: 69 percent / Br2 / CCl4 / 1) r.t., 2) 150 deg C, 1,5 h
View Scheme
参考文献
Kauffmann, Thomas; Fischer, Heinz; Woltermann, Annegret
Chemische Berichte, 1982 , vol. 115, # 2 p. 645 - 653
反应条件
1: 81 percent / tetrahydrofuran / 1) -40 deg C, 2) 30 min, reflux
2: 100 percent / LiAlH4 / tetrahydrofuran / 0 °C
3: 69 percent / Br2 / CCl4 / 1) r.t., 2) 150 deg C, 1,5 h
View Scheme
参考文献
Kauffmann, Thomas; Fischer, Heinz; Woltermann, Annegret
Chemische Berichte, 1982 , vol. 115, # 2 p. 645 - 653
参考文献
Sturniolo; Bellinzoni
Gazzetta Chimica Italiana, 1919 , vol. 49 II, p. 326
反应条件
1: arsenic trichloride / 350 °C
2: alcoholic KOH-solution
View Scheme
参考文献
Pope; Turner
Journal of the Chemical Society, 1920 , vol. 117, p. 1450
参考文献
Sergeew; Gorskii
Zhurnal Obshchei Khimii, 1931 , vol. 1, p. 263,268-271
Chem.Abstr., 1932 , p. 2195
反应条件
diethyl ether; benzene
参考文献
Blicke; Smith
Journal of the American Chemical Society, 1929 , vol. 51, p. 1564
Journal of the American Chemical Society, 1929 , vol. 51, p. 3481
参考文献
Dehn; Wilcox
American Chemical Journal, 1906 , vol. 35, p. 51
反应条件
in tetrahydrofuran
3 h; Heating;
参考文献
Gillespie, Donal G.; Walker, Brian J.; Stevens, David; McAuliffe, Charles A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1697 - 1703
反应条件
in tetrahydrofuran
3 h; Heating;
参考文献
Gillespie, Donal G.; Walker, Brian J.; Stevens, David; McAuliffe, Charles A.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , # 8 p. 1697 - 1703
