4-(4-甲酰基苯氧基)苯甲醛合成路线 （共 16 条）
反应条件
sodium peroxodisulphate; copper diacetate; iron(II) sulfate; dimethyl sulfoxide in water; acetonitrile T=75°C; 0.75 h;
参考文献
TEX-A-TEC AG
Patent: WO2004/43891 A1, 2004 ;
Location in patent: Page 5; 6 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide T=155 - 160°C; 3 h;
参考文献
Dann; Ruff; Wolff; Griessmeier
1984 , vol. 1984, # 3 p. 409 - 425
反应条件
1: 4,4'-dibromodiphenyl ether With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 2 h; 2: N,N-dimethyl-formamide in tetrahydrofuran; hexane T=-78°C; 0.5 h;
参考文献
Kuhnert, Nikolai; Burzlaff, Nicolai; Patel, Chirag; Lopez-Periago, Ana
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 10 p. 1911 - 1921
反应条件
pyridinium chlorochromate in dichloromethane 2 h; Molecular sieveInert atmosphereReflux;
参考文献
Gurung, Santosh K.; Kim, Soo Bae; Park, Haeil
Archives of Pharmacal Research, 2010 , vol. 33, # 12 p. 1919 - 1926
反应条件
lithium tri(t-butoxy)aluminum hydride in tetrahydrofuran T=-78°C; 7.5 h; Yield given;
参考文献
Journal of Heterocyclic Chemistry, , vol. 27, # 4 p. 1007 - 1009
反应条件
pyridine; potassium carbonate; copper(II) oxide T=145 - 150°C; 24 h;
参考文献
Baratov, N. U.; Mil'grom, E. G.; Vinogradova, V. I.; Rashkes, Ya. V.; Yunusov, M. S.
Chemistry of Natural Compounds, 1993 , vol. 29, # 6 p. 748 - 759
Khimiya Prirodnykh Soedinenii, 1993 , # 6 p. 839 - 853
反应条件
1: copper(l) iodide; N,N-dimethylaminoacetic acid; caesium carbonate / 1,4-dioxane / 24 h / Reflux; Inert atmosphere 2: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Cooling with ice; Reflux 3: pyridinium chlorochromate / dichloromethane / 2 h / Molecular sieve; Inert atmosphere; Reflux View Scheme
参考文献
Archives of Pharmacal Research, , vol. 33, # 12 p. 1919 - 1926
反应条件
1: copper(l) iodide; N,N-dimethylaminoacetic acid; caesium carbonate / 1,4-dioxane / 24 h / Reflux; Inert atmosphere 2: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Cooling with ice; Reflux 3: pyridinium chlorochromate / dichloromethane / 2 h / Molecular sieve; Inert atmosphere; Reflux View Scheme
参考文献
Archives of Pharmacal Research, , vol. 33, # 12 p. 1919 - 1926
反应条件
1: sulfuric acid / 4 h / Reflux 2: copper(l) iodide; N,N-dimethylaminoacetic acid; caesium carbonate / 1,4-dioxane / 24 h / Reflux; Inert atmosphere 3: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Cooling with ice; Reflux 4: pyridinium chlorochromate / dichloromethane / 2 h / Molecular sieve; Inert atmosphere; Reflux View Scheme
参考文献
Archives of Pharmacal Research, , vol. 33, # 12 p. 1919 - 1926
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere; Cooling with ice; Reflux 2: pyridinium chlorochromate / dichloromethane / 2 h / Molecular sieve; Inert atmosphere; Reflux View Scheme
参考文献
Archives of Pharmacal Research, , vol. 33, # 12 p. 1919 - 1926
