N,N-二乙基-4-硝基苯胺合成路线 （共 25 条）
反应条件
potassium carbonate in dimethyl sulfoxide T=90°C;
参考文献
KYOTO UNIVERSITY; Kakeya, Hideaki; Hattori, Akira; Takasu, Yasuaki; Fujii, Nobutaka; Oishi, Shinya; Kojima, Soichi; Hara, Mitsuko
Patent: US2013/45977 A1, 2013 ;
Location in patent: Paragraph 0219; 0220; 0221; 0222 ;
反应条件
cerium (IV) oxide; potassium hydroxide in dimethyl sulfoxide T=110°C; Ullmann type coupling; 9 h; Air atmosphere;
参考文献
Agawane, Sandeep M.; Nagarkar, Jayashree M.
Tetrahedron Letters, 2011 , vol. 52, # 41 p. 5220 - 5223
反应条件
potassium carbonate in water T=100°C; Ullmann Condensation; 1 h; Sealed tubeMicrowave irradiation;
参考文献
Nasir Baig; Varma, Rajender S.
RSC Advances, 2014 , vol. 4, # 13 p. 6568 - 6572
反应条件
Bi(NO3)3; sulfuric acid; silica gel T=25°C; 0.0666667 h;
参考文献
Hajipour; Zarei; Ruoho
Russian Journal of Organic Chemistry, 2005 , vol. 41, # 10 p. 1493 - 1495
反应条件
potassium tert-butylate in tert-butyl alcohol T=25°C; Alkylation; Further byproducts given;
参考文献
Angewandte Chemie - International Edition, , vol. 39, # 5 p. 944 - 945
反应条件
iodic acid; sodium nitrite in water T=20°C; 0.0833333 h; chemoselective reaction;
参考文献
Chemistry Letters, , vol. 39, # 8 p. 808 - 809
反应条件
in tetrahydrofuran T=50°C; P=6000480 Torr; 250 h;
参考文献
Ibata, Toshikazu; Isogami, Yasushi; Toyoda, Jiro
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 1 p. 42 - 49
反应条件
ammonium cerium(IV) nitrate in acetonitrile T=20°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 46, # 50 p. 8781 - 8783
反应条件
sodium t-butanolate; PdNaY in toluene T=135°C; Dehydrobromination; amination; 20 h; Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 592, # 2 p. 225 - 234
反应条件
in pyridine T=80°C; 5 h;
参考文献
Matsumura, Eizo; Tohda, Yasuo; Ariga, Masahiro
Bulletin of the Chemical Society of Japan, 1982 , vol. 55, # 7 p. 2174 - 2180
