3-硝基-N,N-二乙基苯胺合成路线 （共 10 条）
反应条件
potassium phosphate; copper(l) iodide; CVT-2537 in dimethyl sulfoxide T=90°C; 16 h; Inert atmosphere;
参考文献
Zhang, Yu; Yang, Xinye; Yao, Qizheng; Ma, Dawei
Organic Letters, 2012 , vol. 14, # 12 p. 3056 - 3059
反应条件
sodium carbonate in ethanol 10 h; Heating;
参考文献
Thiel, W.; Mayer, R.; Jauer, E.-A.; Modrow, H.; Dost, H.
Journal fuer Praktische Chemie (Leipzig), 1986 , vol. 328, # 4 p. 497 - 514
反应条件
sodium t-butanolate; PdNaY in toluene T=135°C; Dehydrobromination; amination; 20 h; Title compound not separated from byproducts;
参考文献
Journal of Organometallic Chemistry, , vol. 592, # 2 p. 225 - 234
参考文献
Journal of the American Chemical Society, , vol. 32, p. 386
Chemische Berichte, , vol. 19, p. 199
反应条件
sulfuric acid; nitric acid
参考文献
Chemische Berichte, , vol. 19, p. 199
参考文献
Zhurnal Organicheskoi Khimii, , vol. 5, # 3 p. 411 - 415,400 - 403
反应条件
sodium acetate; potassium hydrogencarbonate 1.) water, reflux, 36 h, 2.) water, 20 deg C, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 109, p. 337 - 345
反应条件
1: 87 percent / formic acid, triethylamine / 5percent Pd/C / 2.5 h / Heating 2: 77 percent / benzene / 1 h / Heating View Scheme
参考文献
Katritzky, Alan R.; Rachwal, Bogumila; Rachwal, Stanislaw
Recueil des Travaux Chimiques des Pays-Bas, 1990 , vol. 109, p. 337 - 345
反应条件
formic acid; triethylamine; palladium on activated charcoal
2.5 h; Heating;
参考文献
Katritzky, Alan R.; Rachwal, Bogumila; Rachwal, Stanislaw
Recueil des Travaux Chimiques des Pays-Bas, 1990 , vol. 109, p. 337 - 345
反应条件
1: H2 / 5 percent Pd/C / ethanol
2: pyridine
View Scheme
参考文献
Gloster, Daniel F.; Cincotta, Louis; Foley, James W.
Journal of Heterocyclic Chemistry, 1999 , vol. 36, # 1 p. 25 - 32
