N-甲氧基-N,6-二甲基烟酰胺合成路线 （共 12 条）
反应条件
1: 80 percent / tetrahydrofuran; toluene / 1 h / -10 °C 2: 89 percent / sodium tungstate; aq. H2O2 / aq. H2SO4; methanol / 55 °C View Scheme
参考文献
Davies; Marcoux; Corley; Journet; Cai; Palucki; Wu; Larsen; Rossen; Pye; DiMichele; Dormer; Reider
Journal of Organic Chemistry, 2000 , vol. 65, # 25 p. 8415 - 8420
反应条件
1: 80 percent / tetrahydrofuran; toluene / 1 h / -10 °C 2: 89 percent / sodium tungstate; aq. H2O2 / aq. H2SO4; methanol / 55 °C 3: t-BuOK / tetrahydrofuran / 0.75 h / 20 °C 4: AcOH; TFA / tetrahydrofuran / 0.75 h / 25 - 30 °C 5: 8.42 g / aq. NH4OH / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Davies; Marcoux; Corley; Journet; Cai; Palucki; Wu; Larsen; Rossen; Pye; DiMichele; Dormer; Reider
Journal of Organic Chemistry, 2000 , vol. 65, # 25 p. 8415 - 8420
