5,6,7,8-四氢-2-萘胺合成路线 （共 45 条）
参考文献
Journal fuer Praktische Chemie (Leipzig), vol. <2> 142, p. 1935> 153, 169
反应条件
1: 0.5 g / 0.5 h / 260 - 280 °C 2: 83 percent / 10percent Pd/C / various solvent(s) / 8 h / 190 °C 3: 1.) Na, NH3 liq., 2.) AcOH / 1.) THF, 18 h, 2.) 100 deg C to 125 deg C, 18 h View Scheme
参考文献
Rosario, Christopher A.; Holder, Gerald M.; Duke, Colin C.
Journal of Organic Chemistry, 1987 , vol. 52, # 6 p. 1064 - 1072
反应条件
1: 0.5 g / 0.5 h / 260 - 280 °C 2: 83 percent / 10percent Pd/C / various solvent(s) / 8 h / 190 °C 3: 1.) Na, NH3 liq., 2.) AcOH / 1.) THF, 18 h, 2.) 100 deg C to 125 deg C, 18 h 4: 1.) t-BuONa, 2.) DDQ / 1.) t-BuOH, reflux, 15 h, 2.) dioxane, reflux, 15 h View Scheme
参考文献
Rosario, Christopher A.; Holder, Gerald M.; Duke, Colin C.
Journal of Organic Chemistry, 1987 , vol. 52, # 6 p. 1064 - 1072
反应条件
1: 0.5 g / 0.5 h / 260 - 280 °C 2: 83 percent / 10percent Pd/C / various solvent(s) / 8 h / 190 °C 3: 1.) Na, NH3 liq., 2.) AcOH / 1.) THF, 18 h, 2.) 100 deg C to 125 deg C, 18 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 52, # 6 p. 1064 - 1072
反应条件
1: 0.5 g / 0.5 h / 260 - 280 °C 2: 83 percent / 10percent Pd/C / various solvent(s) / 8 h / 190 °C 3: 1.) Na, NH3 liq., 2.) AcOH / 1.) THF, 18 h, 2.) 100 deg C to 125 deg C, 18 h 4: 1.) t-BuONa, 2.) DDQ / 1.) t-BuOH, reflux, 15 h, 2.) dioxane, reflux, 15 h View Scheme
参考文献
Journal of Organic Chemistry, , vol. 52, # 6 p. 1064 - 1072
反应条件
T=260 - 280°C; 0.5 h;
参考文献
Rosario, Christopher A.; Holder, Gerald M.; Duke, Colin C.
Journal of Organic Chemistry, 1987 , vol. 52, # 6 p. 1064 - 1072
反应条件
sulfuric acid Diazotization.Behandlung der Diazoniumsalz-Loesung mit CuBr in wss. HBr;
参考文献
Bassindale,A.R. et al.
Journal of the Chemical Society [Section] B: Physical Organic, 1969 , p. 12 - 15
参考文献
AUCKLAND UNISERVICES LIMITED
Patent: WO2006/104406 A1, 2006 ;
Location in patent: Page/Page column 126 ;
反应条件
in tert-butyl methyl ether T=20°C; 4 h; Molecular sieve;
参考文献
Lal, Samridhi; Snape, Timothy J.
Journal of Molecular Catalysis B: Enzymatic, 2012 , vol. 83, p. 80 - 86
反应条件
diethyl ether; sodium carbonate
参考文献
Sergiewskaja; Wolynskii
Zhurnal Obshchei Khimii, 1952 , vol. 22, p. 1035,1044; engl. Ausg. S. 1085, 1091
