2,3,5,6-四甲基苯胺合成路线 （共 21 条）
反应条件
sulfuric acid Diazotization;
参考文献
Ingham; Hampson
Journal of the Chemical Society, 1939 , p. 981,985
反应条件
methanol; sodium methylate; epoxysulfonyl fluoride; lead dioxide 1.) -78 deg C, 2 h, 2.) -50 deg C to -40 deg C;
参考文献
Rudenko, A. P.; Korovina, N. S.; Aver'yanov, S. F.
Russian Journal of Organic Chemistry, 1995 , vol. 31, # 8 p. 1077 - 1083
Zhurnal Organicheskoi Khimii, 1995 , vol. 31, # 8 p. 1184 - 1190
参考文献
Willstaetter; Kubli
Chemische Berichte, 1909 , vol. 42, p. 4163
反应条件
1: 68 percent Spectr.
2: NH2OH / H2O; pyridine
View Scheme
参考文献
Hagopian, Robert A.; Therien, Michael J.; Murdoch, Joseph R.
Journal of the American Chemical Society, 1984 , vol. 106, # 19 p. 5753 - 5754
反应条件
hydroxylamine in pyridine; water
参考文献
Hagopian, Robert A.; Therien, Michael J.; Murdoch, Joseph R.
Journal of the American Chemical Society, 1984 , vol. 106, # 19 p. 5753 - 5754
反应条件
sodium azide; trifluorormethanesulfonic acid
T=20°C; Ultrasonic irradiation;
参考文献
Borodkin; Elanov; Shubin
Russian Journal of Organic Chemistry, 2009 , vol. 45, # 6 p. 934 - 935
反应条件
ethanol; zinc in water
T=65°C; Title compound not separated from byproducts;
参考文献
Barclay, George G.; Candlin, Jack P.; Lawne, William; Pauson, Peter L.
Journal of Chemical Research, Miniprint, 1992 , p. 2169 - 2187
反应条件
hydrogenchloride; tin(ll) chloride
参考文献
Smith; Taylor
Journal of the American Chemical Society, 1935 , vol. 57, p. 2460,2462
反应条件
hydrogenchloride; tin
参考文献
Smith; Tenenbaum
Journal of the American Chemical Society, 1935 , vol. 57, p. 1293,1295
Full Text Show Details
Birtles; Hampson
Journal of the Chemical Society, 1937 , p. 10,14
Full Text Show Details
Smith; Horner
Journal of the American Chemical Society, 1940 , vol. 62, p. 1349,1353
反应条件
1: concentrated H2SO4; chloroform; HNO3
2: tin; aqueous hydrochloric acid
View Scheme
参考文献
Birtles; Hampson
Journal of the Chemical Society, 1937 , p. 10,14
Full Text Show Details
Smith; Horner
Journal of the American Chemical Society, 1940 , vol. 62, p. 1349,1353
