双(2,4-二硝基苯)二硫化碳合成路线 (共 81 条)
反应条件
in ethanol T=45°C; 48 h; Yields of byproduct given;
参考文献
Cardellini, Mario; Cingolani, Gian Mario; Claudi, Francesco; Gulini, Ugo; Martelli, Sante
Synthesis, 1980 , # 11 p. 886 - 887
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=25°C; 4 h; Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 61, # 4 p. 1533 - 1536
反应条件
in ethanol T=40°C; 52 h; Yields of byproduct given;
参考文献
Cardellini, Mario; Cingolani, Gian Mario; Claudi, Francesco; Gulini, Ugo; Martelli, Sante
Synthesis, 1980 , # 11 p. 886 - 887
反应条件
sodium methylate in methanol T=50°C; 2 h; Further byproducts given;
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 20, p. 1160 - 1167
Zhurnal Organicheskoi Khimii, , vol. 20, # 6 p. 1276 - 1283
反应条件
1: 90 percent / (C16H33)Bu3P(1+)*SCN(1-) / chlorobenzene; H2O / 25 °C 2: tetrabutylammonium halide / chlorobenzene / 60 h View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 461 - 466
参考文献
Journal of the American Chemical Society, , vol. 77, p. 931,933
反应条件
pyridine; 1,2-dichloro-ethane
参考文献
Journal of the American Chemical Society, , vol. 77, p. 6541,6543
反应条件
gallium(III) chloride in tetrahydrofuran T=-5 - 0°C; 0.15 h; further quantitative of reagent, further temperature; Product distribution;
参考文献
Todres, Z. V.; Ovsepyan, G. Ts.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 11 p. 2375 - 2378
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 11 p. 2590 - 2593
反应条件
tetrabutylammonium halide in chlorobenzene 60 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , p. 461 - 466
参考文献
Journal of the Chemical Society, , vol. 125, p. 1379