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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
碘化二苯基碘
合成路线
（共 32 条）
103-19-5
对甲苯二硫醚
+
2217-79-0
碘化二苯基碘
→
反应条件
3699-01-2
4-甲基二苯硫醚
反应条件
1: bis(4-methylphenyl)-disulfide With aluminium trichloride; zinc in acetonitrile T=80°C; 2 h; 2: diphenyliodonium(1+) iodide in water; acetonitrile T=80°C; 4 h;
参考文献
Phosphorus, Sulfur and Silicon and the Related Elements, , vol. 180, # 10 p. 2275 - 2278
2217-79-0
碘化二苯基碘
→
反应条件
3457-58-7
反应条件
1: methanol 2: dimethylformamide View Scheme
参考文献
Kornblum,N.; Taylor,H.J.
Journal of Organic Chemistry, 1963 , vol. 28, p. 1424 - 1425
629-45-8
二丁基二硫
+
2217-79-0
碘化二苯基碘
→
反应条件
1126-80-3
丁基硫基苯
反应条件
1: Di-n-butyl disulfide With aluminium trichloride; zinc in acetonitrile T=80°C; 2 h; 2: diphenyliodonium(1+) iodide in water; acetonitrile T=80°C; 7 h;
参考文献
Movassagh, Barahman; Mossadegh, Amir
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 10 p. 2275 - 2278
822-27-5
二正辛基二硫
+
2217-79-0
碘化二苯基碘
→
反应条件
13910-16-2
反应条件
1: di-n-octyl disulfide With aluminium trichloride; zinc in acetonitrile T=80°C; 2 h; 2: diphenyliodonium(1+) iodide in water; acetonitrile T=80°C; 8.5 h;
参考文献
Movassagh, Barahman; Mossadegh, Amir
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 10 p. 2275 - 2278
5586-15-2
2-萘二硫醚
+
2217-79-0
碘化二苯基碘
→
反应条件
7570-96-9
反应条件
1: NapSSNap With aluminium trichloride; zinc in acetonitrile T=80°C; 2 h; 2: diphenyliodonium(1+) iodide in water; acetonitrile T=80°C; 3 h;
参考文献
Movassagh, Barahman; Mossadegh, Amir
Phosphorus, Sulfur and Silicon and the Related Elements, 2005 , vol. 180, # 10 p. 2275 - 2278
1787-80-0
+
2217-79-0
碘化二苯基碘
→
反应条件
65490-21-3
反应条件
1: bis(naphthalen-1-yl) diselenide With aluminium trichloride; zinc in acetonitrile T=83°C; 2 h; 2: diphenyliodonium(1+) iodide in water; acetonitrile T=83°C; 3.5 h;
参考文献
Movassagh, Barahman; Fazeli, Azadeh
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2006 , vol. 61, # 2 p. 194 - 196
→
反应条件
94800-49-4
反应条件
1: bis(3-methylphenyl) diselenide With aluminium trichloride; zinc in acetonitrile T=83°C; 2 h; 2: diphenyliodonium(1+) iodide in water; acetonitrile T=83°C; 1.5 h;
参考文献
Movassagh, Barahman; Fazeli, Azadeh
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2006 , vol. 61, # 2 p. 194 - 196
20541-49-5
双(4-氯苯基)二硒化物
+
2217-79-0
碘化二苯基碘
→
反应条件
94800-51-8
反应条件
1: (4-ClPhSe)2 With aluminium trichloride; zinc in acetonitrile T=83°C; 2 h; 2: diphenyliodonium(1+) iodide in water; acetonitrile T=83°C; 1.2 h;
参考文献
Movassagh, Barahman; Fazeli, Azadeh
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2006 , vol. 61, # 2 p. 194 - 196
764-93-2
1-癸炔
+
2217-79-0
碘化二苯基碘
→
反应条件
62839-71-8
反应条件
Schwartz's reagent; tetrakis(triphenylphosphine) palladium(0) 1.) THF, room temperature, 2 h, 2.) THF, room temperature, 1.5 h; Yield given. Multistep reaction;
参考文献
Huang, Xian; Sun, Ai-Ming
Synthetic Communications, 1998 , vol. 28, # 5 p. 773 - 778
2217-79-0
碘化二苯基碘
+
104-15-4
对甲苯磺酸
→
反应条件
6293-66-9
对甲苯磺酸盐二溴苯基碘
反应条件
dihydrogen peroxide in ethanol; water Heating;
参考文献
Kazmierczak, Pawel; Skulski, Lech
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 1 p. 219 - 224
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