N,N-二丁基氨基甲酸乙酯合成路线 （共 13 条）
反应条件
lithium aluminium tetrahydride; diethyl ether
参考文献
Dannley et al.
Journal of Organic Chemistry, 1955 , vol. 20, p. 92
反应条件
trichlorophosphate in acetonitrile 15 h; Heating;
参考文献
Hoshino, Osamu; Saito, Keiji; Ishizaki, Miyuki; Umezawa, Bunsuke
Synthetic Communications, 1987 , vol. 17, # 16 p. 1887 - 1892
反应条件
triethylamine in tetrahydrofuran
参考文献
Societe Nationale des Poudres et Explosifs
Patent: US4725680 A1, 1988 ;
反应条件
chlorosulphonyl isocyanate; oxygen; palladium
T=160 - 170°C; 2 h;
参考文献
Fukuoka, Shinsuke; Chono, Masazumi; Kohno, Masashi
Journal of the Chemical Society, Chemical Communications, 1984 , # 6 p. 399 - 400
反应条件
sodium hydroxide; diethyl ether
参考文献
Dannley et al.
Journal of Organic Chemistry, 1955 , vol. 20, p. 92
反应条件
1: dibutylamine; C10H16N2O2 in acetonitrile
T=5°C; 1.5 h;
2: ethyl iodide T=20°C; 6 h;
参考文献
Perez, Eduardo R; Da Silva, Michele Odnicki; Costa, Vanessa C; Rodrigues-Filho, Ubirajara P; Franco, Douglas W
Tetrahedron Letters, 2002 , vol. 43, # 22 p. 4091 - 4093
反应条件
in benzene
2 h; Heating;
参考文献
Cereda, E.; Bellora, E.; Donetti, A.
Tetrahedron Letters, 1980 , vol. 21, p. 4977 - 4980
反应条件
1: carbon dioxide; dibutylamine With potassium carbonate
T=19.84°C; P=760.051 Torr; 2 h;
2: ethyl bromide T=293°C; P=760.051 Torr; 48 h; chemoselective reaction;
参考文献
Kong, De-Lin; He, Liang-Nian; Wang, Jin-Quan
Synthetic Communications, 2011 , vol. 41, # 22 p. 3298 - 3307
反应条件
1: 81 percent / acetonitrile / 18 h / Heating
2: 95 percent / NaOH / H2O
3: 72 percent / benzene / 18 h / Heating
4: 1) triethyloxonium fluoroborate 2) sodium borohydride / 1) methylene dichloride, 25 deg C, 20 hr. 2) ethanol, 0 deg C, 3 hr.
5: benzene / 2 h / Heating
View Scheme
参考文献
Cereda, E.; Bellora, E.; Donetti, A.
Tetrahedron Letters, 1980 , vol. 21, p. 4977 - 4980
反应条件
1: 1) triethyloxonium fluoroborate 2) sodium borohydride / 1) methylene dichloride, 25 deg C, 20 hr. 2) ethanol, 0 deg C, 3 hr.
2: benzene / 2 h / Heating
View Scheme
参考文献
Cereda, E.; Bellora, E.; Donetti, A.
Tetrahedron Letters, 1980 , vol. 21, p. 4977 - 4980
