N,N-二丁基氨基甲酸乙酯合成路线 （共 13 条）
反应条件
1: 72 percent / benzene / 18 h / Heating
2: 1) triethyloxonium fluoroborate 2) sodium borohydride / 1) methylene dichloride, 25 deg C, 20 hr. 2) ethanol, 0 deg C, 3 hr.
3: benzene / 2 h / Heating
View Scheme
参考文献
Cereda, E.; Bellora, E.; Donetti, A.
Tetrahedron Letters, 1980 , vol. 21, p. 4977 - 4980
反应条件
1: 95 percent / NaOH / H2O
2: 72 percent / benzene / 18 h / Heating
3: 1) triethyloxonium fluoroborate 2) sodium borohydride / 1) methylene dichloride, 25 deg C, 20 hr. 2) ethanol, 0 deg C, 3 hr.
4: benzene / 2 h / Heating
View Scheme
参考文献
Cereda, E.; Bellora, E.; Donetti, A.
Tetrahedron Letters, 1980 , vol. 21, p. 4977 - 4980
参考文献
Robson; Reinhart
Journal of the American Chemical Society, 1955 , vol. 77, p. 2453,2455
