N-(3-氨基-4-甲基苯基)苯甲酰胺合成路线 (共 4 条)
反应条件
hydrogenchloride; tin
参考文献
IRM LLC
Patent: WO2006/101783 A2, 2006 ;
Location in patent: Page/Page column 26 ;
WO 2006/101783 A2
反应条件
sodium hydrogencarbonate; triethylamine in diethyl ether; dichloromethane; ethyl acetate
参考文献
AstraZeneca AB
Patent: US6579872 B1, 2003 ;
US 6579872 B1
反应条件
2: tin; hydrochloric acid View Scheme
参考文献
Bell
Chemische Berichte, 1874 , vol. 7, p. 1504
反应条件
1: With methanesulfonic acid in ethanol
19 h; Heating / reflux;
2: With hydrogenchloride; water
3: With sodium hydroxide; sodium carbonate
more than 3 stages;
参考文献
IRM LLC
Patent: WO2005/123719 A1, 2005 ;
Location in patent: Page/Page column 35 ;
WO 2005/123719 A1