2-叔丁基-6-甲基苯酚合成路线 (共 43 条)
反应条件
4-(1-ethenyl)pyridine; oxygen in dimethyl sulfoxide T=60°C; P=7600 Torr; 24 h;
参考文献
Takaki, Ken; Shimasaki, Yohei; Shishido, Tetsuya; Takehira, Katsuomi
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 2 p. 311 - 317
反应条件
phosphate buffer; tyrosinase enzyme in acetonitrile 55 h;
参考文献
Pandey; Muralikrishna; Bhalerao
Tetrahedron Letters, 1990 , vol. 31, # 26 p. 3771 - 3774
反应条件
ammonia; hydrogen in 1,4-dioxane T=230°C; P=760.051 Torr;
参考文献
Bulletin of the Korean Chemical Society, , vol. 33, # 2 p. 387 - 392
反应条件
zinc oxide; sodium hydroxide T=210 - 220°C; 8 h;
参考文献
Krysin; Khlebnikova; Khlebnikov; Pokrovskii; Vasil'ev
Russian Journal of General Chemistry, 2009 , vol. 79, # 6 p. 1156 - 1162
反应条件
cobalt(III) acetate in acetic acid T=70°C; 15 h; other 2,6-di- and 2,4,6-trisubstituted phenols, other temperatures, other times; Product distribution;
参考文献
Hirano, Masao; Ishii, Tadamichi; Morimoto, Takashi
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 4 p. 1434 - 1436
反应条件
perchloric acid; cerium(III) perchlorate; cerium(IV) perchlorate in tetrachloromethane; acetonitrile T=25°C; 1.5 h; var. of ratio, time, solvent; MechanismProduct distribution;
参考文献
Monatshefte fur Chemie, , vol. 129, # 8-9 p. 761 - 768
反应条件
in neat (no solvent) T=79.9 - 179.9°C; effect of temperature; Equilibrium constant;
参考文献
Nesterova; Verevkin; Malova; Pil'shchikov
Journal of applied chemistry of the USSR, 1985 , vol. 58, # 4 pt 1 p. 748 - 754
反应条件
1: conc. HCl / 6 h / 90 - 100 °C
2: aq. KOH, H2 / Raney-nickel / methanol / 1.) 3 - 4 h, RT, 2.) 60 deg C
View Scheme
参考文献
Boehmer, Volker; Stotz, Diethard; Beismann, Klaus; Vogt, Walter
Monatshefte fuer Chemie, 1984 , vol. 115, p. 65 - 78
参考文献
Besev,C. et al.
Acta Chemica Scandinavica (1947-1973), 1963 , vol. 17, p. 2281 - 2284
反应条件
1: 2-(1,1-dimethylethyl)-6-methylphenol With sodium hydroxide
T=130°C; P=25 Torr; 1 h; Autoclave;
2: allyl alcohol T=190°C; 2 h; Autoclave; Further stages;
参考文献
Krysin; Khalikova; Khlebnikova; Nogina; Mamatyuk
Russian Journal of General Chemistry, 2010 , vol. 80, # 11 p. 2290 - 2297