2-叔丁基-6-甲基苯酚合成路线 （共 43 条）
反应条件
sodium hydroxide; ammonia; tetra-(n-butyl)ammonium iodide in dichloromethane; water
1.) 30 min, 2.) 45 deg C, 1 h, 3.) 2.5 h, RT;
参考文献
Menting, Karl-Hans; Eichel, Wolfgang; Riemenschneider, Klaus; Schmand, Horst L. K.; Boldt, Peter
Journal of Organic Chemistry, 1983 , vol. 48, # 17 p. 2814 - 2820
反应条件
1: 2-(1,1-dimethylethyl)-6-methylphenol With potassium carbonate in N,N-dimethyl-formamide
T=20°C; 1 h; Inert atmosphere;
2: methyl iodide in N,N-dimethyl-formamide
T=20°C; Inert atmosphere;
参考文献
Iglesias, Alvaro; Alvarez, Rosana; De-Lera, Angel R.; Muniz, Kilian
Angewandte Chemie - International Edition, 2012 , vol. 51, # 9 p. 2225 - 2228
反应条件
4-Methyl-1,1,3,3-tetrabutylguanidine
T=180°C; 4.5 h;
参考文献
Barcelo, Gerard; Grenouillat, Denis; Senet, Jean-Pierre; Sennyey, Gerard
Tetrahedron, 1990 , vol. 46, # 6 p. 1839 - 1848
反应条件
1: CHCl3
2: diethyl ether
View Scheme
参考文献
Miller,B.
Journal of Organic Chemistry, 1977 , vol. 42, # 8 p. 1402 - 1408
反应条件
1: CHCl3
2: Mg / diethyl ether
View Scheme
参考文献
Miller,B.
Journal of Organic Chemistry, 1977 , vol. 42, # 8 p. 1402 - 1408
反应条件
1: CHCl3
2: Mg / diethyl ether
View Scheme
参考文献
Miller,B.
Journal of Organic Chemistry, 1977 , vol. 42, # 8 p. 1402 - 1408
反应条件
1: CHCl3
2: diethyl ether
View Scheme
参考文献
Miller,B.
Journal of Organic Chemistry, 1977 , vol. 42, # 8 p. 1402 - 1408
参考文献
Miller,B.
Journal of Organic Chemistry, 1977 , vol. 42, # 8 p. 1402 - 1408
反应条件
1: CHCl3
2: Mg / diethyl ether
View Scheme
参考文献
Miller,B.
Journal of Organic Chemistry, 1977 , vol. 42, # 8 p. 1402 - 1408
反应条件
orthophosphorus acid
参考文献
Lemiere, G. L.; Dommisse, R. A.; Alderweireldt, F. C.
Bulletin des Societes Chimiques Belges, 1983 , vol. 92, # 2 p. 195 - 196
