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aniline in 1-methyl-pyrrolidin-2-one; methanol; nitrogen

1: Boc-Phe-Merrifield resin With trifluoroacetic acid in dichloromethane T=20°C; 1 h; 2: phenyl isocyanate in tetrahydrofuran T=60°C; 0.166667 h; microwave irradiation; 3: With triethylamine in tetrahydrofuran; N,N-dimethyl-formamide T=110°C; 0.166667 h; microwave irradiation; Further stages.;