3-苯基-2-氧代己内酰脲合成路线 (共 21 条)
反应条件
sodium hydride in N,N,N',N',N'',N''-hexamethylphosphoric triamide 5 h; Ambient temperature;
参考文献
Fujiwara, Hideji; Bose, Ajay K.; Manhas, Maghar S.; Veen, James M. van der
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1980 , p. 1573 - 1577
反应条件
sodium acetate; acetic acid
参考文献
Bergmann; Delis
Justus Liebigs Annalen der Chemie, 1927 , vol. 458, p. 83
参考文献
Gatewood
Journal of the American Chemical Society, 1925 , vol. 47, p. 2178
反应条件
triethylamine in N,N-dimethyl-formamide
T=20°C;
参考文献
Ley, Steven V.; Massi, Alessandro; Rodriguez, Felix; Horwell, David C.; Lewthwaite, Russell A.; Pritchard, Martyn C.; Reid, Alison M.
Angewandte Chemie - International Edition, 2001 , vol. 40, # 6 p. 1053 - 1055
反应条件
tetra-(n-butyl)ammonium iodide in acetonitrile
T=60 - 80°C; 7 h;
参考文献
Suk-Choong Kim; Byoung-Mog Kwon
Synthesis, 1982 , # 9 p. 795 - 796
反应条件
barium dihydroxide in N,N-dimethyl-formamide
0.0666667 h; Irradiationmicrowave irradiation;
参考文献
Gong; Sohn; Kurth
Journal of Organic Chemistry, 1998 , vol. 63, # 14 p. 4854 - 4856
反应条件
1: 75 percent / triethylamine / benzene
2: sodium hydroxide / H2O / other solvent, other base
View Scheme
参考文献
Kavalek, Jaromir; Machacek, Vladimir; Svobodova, Gabriela; Sterba, Vojeslav
Collection of Czechoslovak Chemical Communications, 1986 , vol. 51, # 2 p. 375 - 390
参考文献
Akeng'a; Read
South African Journal of Chemistry, 2007 , vol. 60, p. 11 - 16
反应条件
1: diethyl ether
2: alcoholic KOH-solution / Behandeln mit alkoh. Salzsaeure
View Scheme
参考文献
Johnson; Hill; Kelsey
Journal of the American Chemical Society, 1920 , vol. 42, p. 1714,1719
反应条件
potassium hydroxide
Behandeln mit alkoh. Salzsaeure;
参考文献
Johnson; Hill; Kelsey
Journal of the American Chemical Society, 1920 , vol. 42, p. 1714,1719