3-甲酰基(1,1-联苯)-4-羧酸合成路线 (共 4 条)
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in water; acetonitrile T=90°C; 12 h;
参考文献
WO2008/28118 A1, ;
Page/Page column 65-66 ;
反应条件
potassium hydrogencarbonate; palladium dichloride in water; N,N-dimethyl-formamide T=85°C; Suzuki-Miyaura Coupling; 24 h; Inert atmosphere;
参考文献
Journal of Physical Organic Chemistry, , vol. 24, # 12 p. 1151 - 1156
反应条件
in N,N-dimethyl-formamide T=20°C; 2 h;
参考文献
WO2008/28118 A1, ;
Page/Page column 65-66 ;
反应条件
1: With 3-chloro-benzenecarboperoxoic acid in dichloromethane Baeyer-Villiger Ketone Oxidation; Inert atmosphere; 2: With potassium hydroxide in methanol; water 1 h;
参考文献
Hathway, Timothy; Chernyshov, Deborah Lipman; Jenks, William S.
Journal of Physical Organic Chemistry, 2011 , vol. 24, # 12 p. 1151 - 1156