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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
22219-02-9
合成路线
（共 33 条）
22219-02-9
→
反应条件
62220-52-4
反应条件
1: thionyl chloride / 5 h / 60 °C 2: 0.5 h / Heating 3: 37 percent / KOH / ethanol / 96 h / Ambient temperature View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
22219-02-9
→
反应条件
62220-53-5
反应条件
1: thionyl chloride / 5 h / 60 °C 2: 0.5 h / Heating 3: 37 percent / KOH / ethanol / 96 h / Ambient temperature 4: 20.1 g / thionyl chloride View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
22219-02-9
→
反应条件
62220-54-6
反应条件
1: thionyl chloride / 5 h / 60 °C 2: 0.5 h / Heating 3: 37 percent / KOH / ethanol / 96 h / Ambient temperature 4: 20.1 g / thionyl chloride 5: 27.0 g / dioxane; H2O / 1 h View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
22219-02-9
→
反应条件
62220-56-8
反应条件
1: thionyl chloride / 5 h / 60 °C 2: 0.5 h / Heating 3: 37 percent / KOH / ethanol / 96 h / Ambient temperature 4: 20.1 g / thionyl chloride 5: 96 percent / dioxane; H2O / 1 h View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
22219-02-9
→
反应条件
62220-57-9
反应条件
1: thionyl chloride / 5 h / 60 °C 2: 0.5 h / Heating 3: 37 percent / KOH / ethanol / 96 h / Ambient temperature 4: 20.1 g / thionyl chloride 5: 27.0 g / dioxane; H2O / 1 h 6: LiAlH4 / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
22219-02-9
→
反应条件
62220-62-6
反应条件
1: thionyl chloride / 5 h / 60 °C 2: 0.5 h / Heating 3: 37 percent / KOH / ethanol / 96 h / Ambient temperature 4: 20.1 g / thionyl chloride 5: 98 percent / triethylamine / acetonitrile / 3 h / Ambient temperature View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
22219-02-9
→
反应条件
62220-63-7
反应条件
1: thionyl chloride / 5 h / 60 °C 2: 0.5 h / Heating 3: 37 percent / KOH / ethanol / 96 h / Ambient temperature 4: 20.1 g / thionyl chloride 5: triethylamine / acetonitrile / 3 h / Ambient temperature View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
22219-02-9
→
反应条件
64465-86-7
反应条件
1: thionyl chloride / 5 h / 60 °C 2: 0.5 h / Heating 3: 37 percent / KOH / ethanol / 96 h / Ambient temperature 4: 20.1 g / thionyl chloride 5: triethylamine / acetonitrile / 3 h / Ambient temperature 6: LiAlH4 View Scheme
参考文献
Brieaddy, Lawrence E.; Hurlbert, B. Stuart; Mehta, Nariman B.
Journal of Organic Chemistry, 1981 , vol. 46, # 8 p. 1630 - 1634
22219-02-9
→
反应条件
38059-09-5
(2-{[2-(羟基甲基)苯基]硫代}苯基)甲醇
反应条件
1: With borane-THF in tetrahydrofuran T=20°C; 16 h; 2: With methanol; water in tetrahydrofuran Product distribution / selectivity;
参考文献
XENON PHARMACEUTICALS INC.
Patent: US2008/234384 A1, 2008 ;
Location in patent: Page/Page column 56 ;
22219-02-9
→
反应条件
3950-02-5
反应条件
thionyl chloride; chlorine in tetrachloromethane
参考文献
Maggiali; Mingiardi; Branca; Ricci
Farmaco, Edizione Scientifica, 1983 , vol. 38, # 12 p. 935 - 939
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