1,3,5-三苯甲酰基-D-呋喃核糖合成路线 （共 36 条）
反应条件
tin(IV) chloride in 1,2-dichloro-ethane 3 h; Ambient temperatureother reagent, reaction time; Product distribution;
参考文献
Nucleosides and Nucleotides, , vol. 16, # 1-2 p. 129 - 144
反应条件
tin(IV) chloride in 1,2-dichloro-ethane 3 h; Ambient temperature; Product distribution;
参考文献
Hanna, Naeem B.; Zajicek, Jaroslav; Piskala, Alois
Nucleosides and Nucleotides, 1997 , vol. 16, # 1-2 p. 129 - 144
反应条件
tin(IV) chloride in 1,2-dichloro-ethane 3 h; Ambient temperature; Product distribution;
参考文献
Nucleosides and Nucleotides, , vol. 16, # 1-2 p. 129 - 144
反应条件
1: 71 percent / CH2N2, BF3*OEt2 / CH2Cl2 / 0.5 h / 4 °C 2: 55 percent / trimethylsilyl trifluoromethanesulfonate / acetonitrile / 0.5 h / Ambient temperature 3: 80 percent / conc. aq. NH4OH / methanol / 24 h View Scheme
参考文献
Ross; Springer; Vasquez; Andrews; Cook; Acevedo
Journal of Heterocyclic Chemistry, 1994 , vol. 31, # 4 p. 765 - 769
反应条件
1: 92 percent / 2,6-lutidine / CH2Cl2 / 10 h / 20 °C 2: 94 percent / SnCl4 / acetonitrile / 20 °C 3: 33 percent / 3,6-dimethyl-9-methylcarbazole; Mg(ClO4)2 / propan-2-ol; H2O / Photolysis View Scheme
参考文献
Wang, Zhiwei; Prudhomme, Daniel R.; Buck, Jason R.; Park, Minnie; Rizzo, Carmelo J.
Journal of Organic Chemistry, 2000 , vol. 65, # 19 p. 5969 - 5985
反应条件
1: 97 percent / 2,6-lutidine / CH2Cl2 / 2.5 h / 20 °C 2: 98 percent / SnCl4 / acetonitrile / 20 °C 3: 52 percent / 3,6-dimethyl-9-ethylcarbazole; Mg(ClO4)2 / propan-2-ol; H2O / 1.5 h / Photolysis View Scheme
参考文献
Park; Rizzo
Journal of Organic Chemistry, 1996 , vol. 61, # 18 p. 6092 - 6093
反应条件
1: 97 percent / 2,6-lutidine / CH2Cl2 / 2.5 h / 20 °C 2: 91 percent / SnCl4 / acetonitrile / 20 °C 3: 53 percent / 9-methylcarbazole; Mg(ClO4)2*6H2O / propan-2-ol; H2O / 25 °C / Photolysis View Scheme
参考文献
Park; Rizzo
Journal of Organic Chemistry, 1996 , vol. 61, # 18 p. 6092 - 6093
反应条件
1: Dess-Martin periodane, MgSO4 / CH2Cl2 2: TiCl4, dimethylaminopyridine, Et3N View Scheme
参考文献
Wolfe; Harry-O'kuru
Tetrahedron Letters, 1995 , vol. 36, # 42 p. 7611 - 7614
反应条件
[bis(2-methoxyethyl)amino]-sulfur trifluoride in dichloromethane T=50°C;
参考文献
Nucleosides, nucleotides and nucleic acids, , vol. 22, # 5-8 p. 1343 - 1346
反应条件
1: 71 percent / CH2N2, BF3*OEt2 / CH2Cl2 / 0.5 h / 4 °C 2: 75 percent / trimethylsilyl trifluoromethanesulfonate / acetonitrile / 0.5 h / Ambient temperature 3: 86 percent / conc. aq. NH4OH / methanol / Ambient temperature View Scheme
参考文献
Ross; Springer; Vasquez; Andrews; Cook; Acevedo
Journal of Heterocyclic Chemistry, 1994 , vol. 31, # 4 p. 765 - 769
