3,5-双三氟甲基苯甲酰胺合成路线 （共 5 条）
反应条件
ammonia in water; toluene T=30°C; 6 h;
参考文献
MITSUBISHI GAS CHEMICAL COMPANY, INC.
Patent: EP1500641 A1, 2005 ;
Location in patent: Page 11 ;
反应条件
triphenylphosphine; palladium diacetate in hexane; ethyl acetate; N,N-dimethyl-formamide
反应条件
palladium diacetate in tetrahydrofuran; ethyl acetate
反应条件
N-methyl-2-(methylamino)ethylamine; copper(l) iodide in toluene T=140°C; 16 h;
参考文献
Schareina, Thomas; Zapf, Alexander; Maegerlein, Wolfgang; Mueller, Nikolaus; Beller, Matthias
Chemistry - A European Journal, 2007 , vol. 13, # 21 p. 6249 - 6254
反应条件
1: With tetrachloromethane; triphenylphosphine in tetrahydrofuran T=60°C; 3 h; 2: With phosphorus pentoxide in tetrahydrofuran
参考文献
MITSUBISHI GAS CHEMICAL COMPANY, INC.
Patent: EP1500641 A1, 2005 ;
Location in patent: Page 11 ;
