4-苄氧基-3-甲氧基苯乙胺合成路线 （共 39 条）
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 2 h; Reflux;
参考文献
SHANGHAI INSTITUTE OF MATERIA MEDICA, CHINESE ACADEMY OF SCIENCES; LIU, Hong; XIE, Xin; ZHEN, Xuechu; SUN, Haifeng; LI, Jing; ZHU, Liyuan; LI, Zeng; CHEN, Ying; JIANG, Hualiang; CHEN, Kaixian
Patent: US2014/88130 A1, 2014 ;
Location in patent: Paragraph 0087 ;
反应条件
trifluoroacetic acid T=0°C; 0.666667 h;
参考文献
European Journal of Medicinal Chemistry, , vol. 43, # 6 p. 1160 - 1170
反应条件
samarium diiodide; water; isopropylamine in tetrahydrofuran
参考文献
Ankner, Tobias; Hilmersson, Goeran
Tetrahedron Letters, 2007 , vol. 48, # 32 p. 5707 - 5710
反应条件
1: 96 percent / AcOH; ethylenediamine / 20 °C 2: 96 percent / LAH / tetrahydrofuran / 24 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 71, # 25 p. 9440 - 9448
反应条件
1: With lithium aluminium tetrahydride in diethyl ether 30 h; Heating; 2: With sodium hydroxide in diethyl ether; water 0.5 h; cooling;
参考文献
Reimann, Eberhard; Grasberger, Fritz
Monatshefte fur Chemie, 2005 , vol. 136, # 2 p. 193 - 209
反应条件
1: aq. KOH / ethanol 2: MeNH2*HCl, Na2CO3 / ethanol 3: LiAlH4 / tetrahydrofuran View Scheme
参考文献
Tetrahedron, , vol. 23, p. 2563 - 2570
反应条件
1.1: sodium hydride / tetrahydrofuran; mineral oil / 10 - 20 °C / Inert atmosphere 1.2: 18 h / Reflux; Inert atmosphere 2.1: ammonium acetate / acetic acid / 5 h / Inert atmosphere; Reflux 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 10 °C / Inert atmosphere; Reflux View Scheme
参考文献
Arkivoc, , vol. 2011, # 5 p. 167 - 179
参考文献
Zhurnal Obshchei Khimii, , vol. 29, p. 3831,3834;engl.Ausg.S.3793,3795
反应条件
1: K2CO3 / ethanol / Heating 2: NH4OAc; AcOH / Heating 3: LiAlH4 / diethyl ether; tetrahydrofuran / Heating View Scheme
参考文献
Journal of Medicinal Chemistry, , vol. 45, # 23 p. 5058 - 5068
反应条件
1: dimethylformamide 2: LiAlH4 / diethyl ether View Scheme
参考文献
Phytochemistry (Elsevier), , vol. 24, # 3 p. 469 - 472
