5-溴-2-异丁氧基苯甲醛合成路线 （共 2 条）
反应条件
potassium carbonate in N,N-dimethyl-formamide T=75 - 80°C; 2 h;
参考文献
WO2011/73617 A1, ;
Page/Page column 26 ;
反应条件
1.1: hydroxylamine hydrochloride; sodium formate / formic acid / 7 h / 99 - 100 °C 2.1: n-butyllithium / hexane; tetrahydrofuran / 3 h / -45 - -40 °C 2.2: -20 °C 3.1: sodium carbonate / tetrakis(triphenylphosphine) palladium(0) / toluene; water / 1 h / 70 - 75 °C View Scheme
参考文献
CIPLA LIMITED; BIRARI, Dilip, Ramdas; RAO, Dharmaraj, Ramachandra; KANKAN, Rajendra, Narayanrao; CURTIS, Philip, Anthony
Patent: WO2011/73617 A1, 2011 ;
