3,4',5-三甲氧基-反-二苯代乙烯合成路线 （共 14 条）
反应条件
methanesulfonyl chloride; triethylamine in toluene T=0 - 80°C; 4.5 - 8.5 h;
参考文献
EP1884508 A1, ;
Page/Page column 6 ;
参考文献
Phytochemistry, , vol. 42, # 2 p. 283 - 286
反应条件
1: 3,5-dimethoxybenzyl 3,5-bis(trifluoromethyl)phenyl sulfone With potassium hydroxide; tetrabutylammomium bromide in tetrahydrofuran 0.5 h; 2: 4-methoxy-benzaldehyde in tetrahydrofuran T=20°C; Julia-Kocienski olefination; 16 h;
参考文献
Journal of Organic Chemistry, , vol. 70, # 16 p. 6404 - 6416
反应条件
sodium methylate in N,N-dimethyl-formamide T=20°C; Wittig reaction; 10 h;
参考文献
Free Radical Research, , vol. 45, # 11-12 p. 1379 - 1387
反应条件
1.1: MnSO4*H2O; H2O2; NaHCO3 buffer / acetonitrile / 20 °C 2.1: KOH; tetrabutylammonium bromide / tetrahydrofuran / 0.5 h 2.2: 81 percent / tetrahydrofuran / 16 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 70, # 16 p. 6404 - 6416
反应条件
1.1: NaH / acetonitrile / 24 h / 20 °C 2.1: MnSO4*H2O; H2O2; NaHCO3 buffer / acetonitrile / 20 °C 3.1: KOH; tetrabutylammonium bromide / tetrahydrofuran / 0.5 h 3.2: 81 percent / tetrahydrofuran / 16 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 70, # 16 p. 6404 - 6416
反应条件
1: hydrogenchloride / benzene / 3.5 h / 0 °C 2: Reflux 3: sodium methylate / N,N-dimethyl-formamide / 10 h / 20 °C View Scheme
参考文献
Free Radical Research, , vol. 45, # 11-12 p. 1379 - 1387
反应条件
1: Reflux 2: sodium methylate / N,N-dimethyl-formamide / 10 h / 20 °C View Scheme
参考文献
Free Radical Research, , vol. 45, # 11-12 p. 1379 - 1387
参考文献
Food Chemistry, , vol. 135, # 3 p. 1011 - 1019
反应条件
1: acetic anhydride; triethylamine 2: copper; quinoline View Scheme
参考文献
Food Chemistry, , vol. 135, # 3 p. 1011 - 1019
