反应条件
n-butyl lithium; H2O in diethyl ether; hexane
addn. of n-BuLi soln. (hexane) to ferrocene soln. (Et2O) under Ar; addn. of Si compd. by syringe; stirring, 35°C, 45 min; cooling; hydrolysing (cold H2O); extn. (Et2O); drying (MgSO4); filtration; evapn.; chromy. (silica gel, hexane);
参考文献
Borgdorff, Jan; Ditzel, Evert J.; Duffy, Noel W.; Robinson, Brian H.; Simpson, Jim
Journal of Organometallic Chemistry, 1992 , vol. 437, # 3 p. 323 - 346
