3-(4-甲氧基苯基)丙酸合成路线 (共 50 条)
反应条件
potassium acetate; palladium diacetate; silver(l) oxide in dichloromethane T=20°C; 12 h; Molecular sieve;
参考文献
Feng, Chao; Loh, Teck-Peng
Chemical Communications, 2010 , vol. 46, # 26 p. 4779 - 4781
反应条件
copper(l) iodide; potassium carbonate; triphenylphosphine in dimethyl sulfoxide T=90°C; 24 h; Inert atmosphere;
参考文献
Qu, Xiaoming; Li, Tingyi; Sun, Peng; Zhu, Yan; Yang, Hailong; Mao, Jincheng
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 20 p. 6938 - 6942
反应条件
P2O5; methanesulfonic acid 12 h; Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 55, # 14 p. 4349 - 4356
参考文献
Hariharan; Sudborough
Journal of the Indian Institute of Science, 1925 , vol. <A> 8, p. 216
Chem. Zentralbl., 1926 , vol. 97, # I p. 72
反应条件
1: thionyl chloride / 16 h
2: AlCl3 / CH2Cl2 / 1 h / -78 °C
View Scheme
参考文献
Wadsworth, Donald H.; Geer, Susan M.; Detty, Michael R.
Journal of Organic Chemistry, 1987 , vol. 52, # 16 p. 3662 - 3668
反应条件
copper(l) iodide; potassium carbonate; triphenylphosphine in dimethyl sulfoxide
T=100°C; 24 h; Inert atmosphere;
参考文献
Li, Tingyi; Sun, Peng; Yang, Hailong; Zhu, Yan; Yan, Hong; Lu, Linhua; Mao, Jincheng
Tetrahedron, 2012 , vol. 68, # 32 p. 6413 - 6419
反应条件
copper(l) iodide; potassium carbonate; triphenylphosphine in dimethyl sulfoxide
T=100°C; 24 h; Inert atmosphere;
参考文献
Li, Tingyi; Sun, Peng; Yang, Hailong; Zhu, Yan; Yan, Hong; Lu, Linhua; Mao, Jincheng
Tetrahedron, 2012 , vol. 68, # 32 p. 6413 - 6419
反应条件
C16H14N2O4Pd; silver(l) oxide in dichloromethane
T=20°C; 12 h;
参考文献
Heo, Yumi; Kang, Yi Young; Palani, Thiruvengadam; Lee, Junseong; Lee, Sunwoo
Inorganic Chemistry Communications, 2012 , vol. 23, p. 1 - 5
反应条件
in 1-methyl-pyrrolidin-2-one
T=80°C; 14 h;
参考文献
Tartaggia, Stefano; De Lucchi, Ottorino; Goossen, Lukas J.
European Journal of Organic Chemistry, 2012 , # 7 p. 1431 - 1438
参考文献
Vasilyev; Fundamenskii; Savchenkov; Rudenko
Russian Journal of Organic Chemistry, 2003 , vol. 39, # 6 p. 860 - 862