2-溴-3'-硝基苯乙酮合成路线 （共 50 条）
反应条件
N-bromosuccinmide; tetrachlorosilane in acetonitrile T=20°C; 7 h;
参考文献
Salama, Tarek A.; Novak, Zoltan
Tetrahedron Letters, 2011 , vol. 52, # 31 p. 4026 - 4029
反应条件
water; silver fluoride; trifluoroacetic acid T=40°C; 6 h; Green chemistry;
参考文献
Chen, Zheng-Wang; Ye, Dong-Nai; Ye, Min; Zhou, Zhong-Gao; Li, Shen-Huan; Liu, Liang-Xian
Tetrahedron Letters, 2014 , vol. 55, # 7 p. 1373 - 1375
反应条件
N-bromosuccinmide; silica gel in methanol 0.283333 h; Reflux; chemoselective reaction;
参考文献
Mohan Reddy, Bodireddy; Venkata Ramana Kumar, Velpula; Chinna Gangi Reddy, Nallagondu; Mahender Rao, Siripragada
Chinese Chemical Letters, 2014 , vol. 25, # 1 p. 179 - 182
反应条件
Oxonereg;; NH4Br 3 h; Reflux; regioselective reaction;
参考文献
Tetrahedron Letters, , vol. 53, # 2 p. 191 - 195
反应条件
sulfuric acid; nitric acid T=-20°C;
参考文献
Journal of the American Chemical Society, , vol. 56, p. 1369
反应条件
Sodium bromate; sulfuric acid; sodium bromide in 1,4-dioxane; water T=20°C; 15 h;
参考文献
Tetrahedron Letters, , vol. 50, # 21 p. 2529 - 2532
反应条件
1: sulfuric acid; nitric acid / 0.25 h / -5 - 5 °C 2: bromine / acetic acid / 0.5 h / 55 °C View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 67, p. 142 - 151
参考文献
Journal of the Chemical Society, , p. 2416,2422
参考文献
Chemische Berichte, , vol. 10, p. 2010
反应条件
1: 95 percent / CHCl3 / 24 h 2: 90 percent / conc. HCl / aq. ethanol / 72 h View Scheme
参考文献
Imperial Chemical Industries PLC
Patent: US4423045 A1, 1983 ;
