2-溴-3'-硝基苯乙酮合成路线 （共 50 条）
反应条件
1: 98 percent / acetone / 25 °C 2: 55 percent / H2 / 10percent Pd/C / ethanol / 2.5 h View Scheme
参考文献
Collins, Jon L.; Shearer, Barry G.; Oplinger, Jeffrey A.; Lee, Shuliang; Garvey, Edward P.; Salter, Mark; Duffy, Claire; Burnette, Thimysta C.; Furfine, Eric S.
Journal of Medicinal Chemistry, 1998 , vol. 41, # 15 p. 2858 - 2871
反应条件
in ethanol 5 h; RefluxInert atmosphere;
参考文献
IMPACT THERAPEUTICS, INC.; CAI, Suixiong; TIAN, Ye Edward; KANG, Sishun; MENG, Zheng; GU, Chengyun; YIN, Feng; CHEN, Shengzhi; ZHANG, Yang; ZHANG, Xiuyan; FEI, Hongqiang; WANG, Dongmei
Patent: WO2014/12511 A1, 2014 ;
Location in patent: Page/Page column 55 ;
反应条件
sodium disulfite; hydrogen bromide in acetic acid 3 h; Heating;
参考文献
Choi, Han Young; Chi, Dae Yoon
Organic Letters, 2003 , vol. 5, # 4 p. 411 - 414
反应条件
in ethanol 4 h; Heating;
参考文献
Saddik; Khoutoul; Benchat; Hammouti; S. El Kadiri; Touzani
Research on Chemical Intermediates, 2012 , vol. 38, # 9 p. 2457 - 2470
反应条件
1: NaBH4; 2-(3-NO2-Ph)-1,3,2-dioxaborolane-(4R,5R)-dicarboxylic acid / tetrahydrofuran / 25 °C 2: aq. NaOH / tetrahydrofuran / 25 °C View Scheme
参考文献
Cordes, David B.; Kwong, Tracey J.; Morgan, Kellie A.; Singaram, Bakthan
Tetrahedron Letters, 2006 , vol. 47, # 3 p. 349 - 351
反应条件
in water; N,N-dimethyl-formamide
T=25°C; 0.75 h;
参考文献
Carabateas; Brundage; Gelotte; et al.
Journal of Heterocyclic Chemistry, 1984 , vol. 21, # 6 p. 1849 - 1856
参考文献
Bahner et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 4011
参考文献
Bahner et al.
Journal of the American Chemical Society, 1951 , vol. 73, p. 3499
参考文献
Bahner et al.
Journal of the American Chemical Society, 1952 , vol. 74, p. 4198
参考文献
Kunckell
Chemische Berichte, 1897 , vol. 30, p. 576
