4-(叔丁基)-1-环己烯合成路线 （共 72 条）
反应条件
tri-n-butyl-tin hydride; lithium chloride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran 24 h; Heating;
参考文献
Scott, William J.; Crisp, G. T.; Stille, J. K.
Journal of the American Chemical Society, 1984 , vol. 106, # 16 p. 4630 - 4632
反应条件
tri-n-butyl-tin hydride; lithium chloride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=50°C; P=2280 Torr;
参考文献
Journal of the American Chemical Society, , vol. 108, p. 452
反应条件
tri-n-butyl-tin hydride; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=50°C; P=2280 Torr;
参考文献
Journal of the American Chemical Society, , vol. 108, p. 452
反应条件
in 1-methyl-pyrrolidin-2-one
参考文献
Bennani, Youssef L.; Chang, Sou-Jen; Chemburkar, Sanjay R.; Dart, Michael J.; Fernando, Dilinie P.; Grieme, Timothy A.
Patent: US2004/209859 A1, 2004 ;
反应条件
tetrachloromethane; triphenylphosphine 6 h; Heating;
参考文献
Australian Journal of Chemistry, , vol. 36, # 11 p. 2123 - 2132
反应条件
pyridine in diethyl ether T=0°C;
参考文献
Journal of the American Chemical Society, , vol. 109, p. 7838
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene T=100°C; 24 h;
参考文献
Aciro, Caroline; Claridge, Timothy D. W.; Davies, Stephen G.; Roberts, Paul M.; Russell, Angela J.; Thomson, James E.
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 20 p. 3751 - 3761
反应条件
chloro-trimethyl-silane; sodium iodide in acetonitrile 0.333333 h; Ambient temperature;
参考文献
Caputo, Romualdo; Mangoni, Lorenzo; Neri, Orsola; Palumbo, Giovanni
Tetrahedron Letters, 1981 , vol. 22, # 36 p. 3551 - 3552
反应条件
pyridine; trichlorophosphate T=0 - 20°C; 24 h;
参考文献
Aciro, Caroline; Claridge, Timothy D. W.; Davies, Stephen G.; Roberts, Paul M.; Russell, Angela J.; Thomson, James E.
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 20 p. 3751 - 3761
反应条件
1: 75 percent / KOMe, 18-crown-6 / tetrahydrofuran 2: 61 percent / K2CO3 / aq. ethanol / 48 h 3: pyridine / diethyl ether / 0 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 109, p. 7838
