4-(叔丁基)-1-环己烯合成路线 (共 72 条)
反应条件
1: 61 percent / K2CO3 / aq. ethanol / 48 h 2: pyridine / diethyl ether / 0 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 109, p. 7838
反应条件
triethylamine; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; triphenyl-arsane in 1,4-dioxane T=80°C; Borylation; 16 h; Title compound not separated from byproducts;
参考文献
Synthesis, , # 6 p. 778 - 780
反应条件
N,N'-dicyclohexyl-N-methylcarbodiimidium iodide in tetrahydrofuran T=25°C;
参考文献
Tetrahedron, , vol. 50, # 8 p. 2415 - 2432
反应条件
lithium aluminium deuteride; CoAlx in tetrahydrofuran T=65°C; 48 h; reduction with CoAlx and LiAlD4 with other substrate, inversion and retention; Product distribution;
参考文献
Journal of the American Chemical Society, , vol. 108, # 1 p. 67 - 72
反应条件
potassium tert-butylate in dimethyl sulfoxide T=70°C; 1.5 h; Yield given;
参考文献
Journal of Organometallic Chemistry, , vol. 389, # 2 p. 149 - 157
反应条件
chloro-trimethyl-silane; mercury; zinc in diethyl ether 17 h; Heating; Yields of byproduct given;
参考文献
Motherwell, William B.; O'Mahony, Donogh J.R.; Popkin, Matthew E.
Tetrahedron Letters, 1998 , vol. 39, # 29 p. 5285 - 5288
反应条件
chloro-trimethyl-silane; mercury; zinc in diethyl ether 14 h; Heating; Yields of byproduct given;
参考文献
Motherwell, William B.; O'Mahony, Donogh J.R.; Popkin, Matthew E.
Tetrahedron Letters, 1998 , vol. 39, # 29 p. 5285 - 5288
反应条件
bis(acetylacetonato) palladium; n-butyllithium in tetrahydrofuran; hexane Heating;
参考文献
Gai, Yonghua; Jin, Liren; Julia, Marc; Verpeaux, Jean-Noel
Journal of the Chemical Society, Chemical Communications, 1993 , # 21 p. 1625 - 1626
反应条件
.alpha.,.alpha.,.alpha.-trichloroacetamide; triphenylphosphine in dichloromethane T=30°C; 0.25 h;
参考文献
Tetrahedron Letters, , vol. 47, # 38 p. 6821 - 6823
反应条件
T=208°C; unter vermindertem Druck;
参考文献
Journal of the American Chemical Society, , vol. 77, p. 5562,5577