3-乙基-4-甲基-3-戊烯-2-酮合成路线 （共 15 条）
反应条件
1: hexane; acetyl chloride; AlCl3 2: sodium hypobromite View Scheme
参考文献
Nenitzescu; Chicos
Chemische Berichte, 1935 , vol. 68, p. 1587
反应条件
T=280°C; P=2206520 Torr;
参考文献
Hogsed; Lindsey
Journal of the American Chemical Society, 1954 , vol. 76, p. 2305
反应条件
BF3*AcOH in chloroform-d1
T=70°C; 0.25 h; Yield given;
参考文献
Fleming, Ian; Perry, David A.
Tetrahedron, 1981 , vol. 37, # 23 p. 4027 - 4034
反应条件
1: 92 percent / TiCl4 / CH2Cl2 / 2 h / -78 °C
2: 1.) m-chloroperbenzoic acid / 1.) CH2Cl2, -78 deg C, 10 min, 2.) CCl4, reflux
3: BF3*AcOH / CDCl3 / 0.25 h / 70 °C
View Scheme
参考文献
Fleming, Ian; Perry, David A.
Tetrahedron, 1981 , vol. 37, # 23 p. 4027 - 4034
反应条件
tin(IV) chloride
Ambient temperature;
参考文献
Dubois, Jacques-Emile; Saumtally, Imran; Lion, Claude
Bulletin de la Societe Chimique de France, 1984 , vol. 2, # 3-4 p. 133 - 138
反应条件
T=280°C; P=2206520 Torr;
参考文献
Hogsed; Lindsey
Journal of the American Chemical Society, 1954 , vol. 76, p. 2305
反应条件
in acetic anhydride
T=125°C; 0.0833333 h; Yield given. Yields of byproduct given;
参考文献
Loiseau, Andre-Michel; Luft, Robert; Zunino, Serge
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 5-6 p. 144 - 152
反应条件
in acetic anhydride
T=125°C; 0.0833333 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Loiseau, Andre-Michel; Luft, Robert; Zunino, Serge
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 5-6 p. 144 - 152
反应条件
in acetic anhydride
T=125°C; 0.0833333 h; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Loiseau, Andre-Michel; Luft, Robert; Zunino, Serge
Bulletin de la Societe Chimique de France, 1982 , vol. 2, # 5-6 p. 144 - 152
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide
Irradiation;
参考文献
Ono,N. et al.
Chemistry Letters, 1977 , p. 189 - 190
