3-亚甲基-2,6-庚烷二酮合成路线 (共 42 条)
反应条件
H-ZSM-5 zeolite in benzene T=199.9°C; 5 h; Yield given. Yields of byproduct given;
参考文献
Reddy, P. Veera; Prakash, Adekkanattu M.; Chakrabarty, Dipak K.; Bhat, Sujata V.
Journal of Chemical Research, Synopses, 1997 , # 8 p. 306 - 307
反应条件
H-ZSM-5 zeolite in benzene T=199.9°C; 5 h; Yield given. Yields of byproduct given;
参考文献
Reddy, P. Veera; Prakash, Adekkanattu M.; Chakrabarty, Dipak K.; Bhat, Sujata V.
Journal of Chemical Research, Synopses, 1997 , # 8 p. 306 - 307
反应条件
octanol; 1,4-diaza-bicyclo[2.2.2]octane
T=20°C; Baylis-Hillman reaction; 12 h;
参考文献
Park, Kwang-Su; Kim, Jinyoung; Choo, Hyunah; Chong, Youhoon
Synlett, 2007 , # 3 p. 395 - 398
反应条件
methyl(diphenyl)-phosphine in acetonitrile
T=20°C; 36 h; Molecular sieveInert atmosphere;
参考文献
Ma, Guang-Ning; Wang, Fei-Jun; Gao, Jun; Shi, Min
Chemical Communications, 2008 , # 40 p. 4998 - 5000
反应条件
methyl(diphenyl)-phosphine in acetonitrile
T=20°C; 48 h; Molecular sieveInert atmosphere;
参考文献
Ma, Guang-Ning; Wang, Fei-Jun; Gao, Jun; Shi, Min
Chemical Communications, 2008 , # 40 p. 4998 - 5000
反应条件
methyl(diphenyl)-phosphine in acetonitrile
T=20°C; 48 h; Molecular sieveInert atmosphere;
参考文献
Ma, Guang-Ning; Wang, Fei-Jun; Gao, Jun; Shi, Min
Chemical Communications, 2008 , # 40 p. 4998 - 5000
反应条件
methyl(diphenyl)-phosphine in acetonitrile
T=20°C; 48 h; Molecular sieveInert atmosphere;
参考文献
Ma, Guang-Ning; Wang, Fei-Jun; Gao, Jun; Shi, Min
Chemical Communications, 2008 , # 40 p. 4998 - 5000
反应条件
(.eta.5-C5Me5)RuH3(PCy3) in tetrahydrofuran
T=80°C; 24 h;
参考文献
Yi, Chae S.; Liu, Nianhong
Journal of Organometallic Chemistry, 1998 , vol. 553, # 1-2 p. 157 - 161
反应条件
[Rh(H)(PEt3)3] in isopropyl alcohol
T=40°C; 40 h;
参考文献
Sato, Susumu; Matsuda, Isamu; Shibata, Masahiro
Journal of Organometallic Chemistry, 1989 , vol. 377, p. 347 - 356
反应条件
1,4-diaza-bicyclo[2.2.2]octane in N,N-dimethyl-formamide
T=20°C; Baylis-Hillman reaction; 49 h;
参考文献
Shi, Min; Li, Chao-Qun; Jiang, Jian-Kang
Tetrahedron, 2003 , vol. 59, # 8 p. 1181 - 1189