5-氨基-6-羟基烟酸甲酯合成路线 （共 3 条）
反应条件
hydrogen; palladium on activated charcoal in ethanol 23 h; Yield given;
参考文献
Linn, James A.; Gerritz, Samuel W.; Handlon, Anthony L.; Hyman, Clifton E.; Heyer, Dennis
Tetrahedron Letters, 1999 , vol. 40, # 12 p. 2227 - 2230
反应条件
1: 48 percent / red fuming HNO3 / 70 - 80 °C 2: pyridine, SOCl2 / acetonitrile / 2 h / Heating 3: Et3N / acetonitrile / 2 h / Ambient temperature 4: H2 / 10 percent Pd/C / aq. ethanol / 23 h View Scheme
参考文献
Linn, James A.; Gerritz, Samuel W.; Handlon, Anthony L.; Hyman, Clifton E.; Heyer, Dennis
Tetrahedron Letters, 1999 , vol. 40, # 12 p. 2227 - 2230
反应条件
1: pyridine, SOCl2 / acetonitrile / 2 h / Heating 2: Et3N / acetonitrile / 2 h / Ambient temperature 3: H2 / 10 percent Pd/C / aq. ethanol / 23 h View Scheme
参考文献
Linn, James A.; Gerritz, Samuel W.; Handlon, Anthony L.; Hyman, Clifton E.; Heyer, Dennis
Tetrahedron Letters, 1999 , vol. 40, # 12 p. 2227 - 2230
