(S)-1-溴-3-甲基戊烷合成路线 (共 7 条)
反应条件
bromine; triphenylphosphine in tetrachloromethane
参考文献
Chattopadhyay; Chadha; Mamdapur
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 2 p. 247 - 249
反应条件
lithium bromide in acetone Ambient temperature; Yield given;
参考文献
Zhou; Lu; Chen; Yang
Chemistry of Natural Compounds, 2010 , vol. 46, # 1 p. 83 - 85
反应条件
sulfuric acid; hydrogen bromide
参考文献
Couture,A. et al.
Journal of the American Chemical Society, 1976 , vol. 98, p. 6218 - 6225
反应条件
1: 90 percent / LAH / diethyl ether 2: 80 percent / triphenylphosphine, bromine / CCl4 View Scheme
参考文献
Chattopadhyay; Chadha; Mamdapur
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1991 , vol. 30, # 2 p. 247 - 249
反应条件
2: (i) O3, (ii) LiAlH4 View Scheme
参考文献
Salvadori,P. et al.
Tetrahedron Letters, 1977 , p. 195 - 198
反应条件
(i) Mg, (ii) /BRN= 1900390/, Et2O; Multistep reaction;
参考文献
Rezanka, Tomas; Sigler, Karel
European Journal of Organic Chemistry, 2006 , # 18 p. 4277 - 4284
反应条件
1.1: Mg / tetrahydrofuran / 6 h / Heating
1.2: tetrahydrofuran
2.1: methanol / diethyl ether
View Scheme
参考文献
Rezanka, Tomas; Sigler, Karel
European Journal of Organic Chemistry, 2006 , # 18 p. 4277 - 4284