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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
22317-35-7
合成路线
（共 20 条）
1252675-90-3
→
反应条件
22317-35-7
反应条件
sodium hydroxide in tetrahydrofuran; water T=20°C; 16 h;
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
7382-68-5
→
反应条件
22317-35-7
+
90-05-1
愈创木酚
+
498-02-2
4'-羟基-3'-甲氧基苯乙酮
反应条件
Ru(H)2(CO)(PPh3)(xantphos) in deuterated toluene T=135°C; P=760.051 Torr; 20 h; Inert atmosphere;
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
99634-01-2
→
反应条件
22317-35-7
反应条件
1: Ru(H)2(CO)(PPh3)(xantphos) / deuterated toluene / 2 h / 135 °C / 760.05 Torr / |Inert atmosphere 2: potassium carbonate / acetone / 16 h / 20 °C 3: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
14385-48-9
→
反应条件
22317-35-7
反应条件
1: RuH2(CO)(PPh3)3; hydrogen / deuterated toluene / 20 h / 135 °C / 760.05 Torr 2: potassium carbonate / acetone / 16 h / 20 °C 3: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
77891-30-6
→
反应条件
22317-35-7
反应条件
1: Ru(H)2(CO)(PPh3)(xantphos) / deuterated toluene / 2 h / 135 °C / 760.05 Torr / |Inert atmosphere 2: potassium carbonate / acetone / 16 h / 20 °C 3: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
78405-40-0
→
反应条件
22317-35-7
反应条件
1: Ru(H)2(CO)(PPh3)(xantphos) / deuterated toluene / 20 h / 135 °C / 760.05 Torr / |Inert atmosphere 2: potassium carbonate / acetone / 16 h / 20 °C 3: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
186255-41-4
→
反应条件
22317-35-7
反应条件
1: RuH2(CO)(PPh3)3; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; hydrogen / deuterated toluene / 20 h / 135 °C / 760.05 Torr 2: potassium carbonate / acetone / 16 h / 20 °C 3: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
90-05-1
愈创木酚
→
反应条件
22317-35-7
反应条件
1: potassium carbonate / acetone / 16 h / 20 °C 2: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
498-02-2
4'-羟基-3'-甲氧基苯乙酮
→
反应条件
22317-35-7
反应条件
1.1: copper(I) bromide / ethanol 2.1: sodium / ethanol 2.2: Cooling with ice View Scheme
参考文献
Song, Qi; Wang, Feng; Xu, Jie
Chemical Communications, 2012 , vol. 48, # 56 p. 7019 - 7021
102834-26-4
→
反应条件
22317-35-7
反应条件
1: potassium carbonate / acetone / 16 h / 20 °C 2: sodium hydroxide / tetrahydrofuran; water / 16 h / 20 °C View Scheme
参考文献
Wu, Adam; Patrick, Brian O.; Chung, Enoch; James, Brian R.
Dalton Transactions, 2012 , vol. 41, # 36 p. 11093 - 11106
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