1,3-二碘-5,5-二甲基海因合成路线 （共 2 条）
反应条件
sodium hydroxide; iodine cloride in chloroform T=0°C; 0.25 h;
参考文献
Raab, Conrad E.; Dean, Dennis C.; Melillo, David G.
Journal of Labelled Compounds and Radiopharmaceuticals, 2001 , vol. 44, # 12 p. 815 - 829
反应条件
in acetic acid n-butyl ester; water
T=40 - 110°C; P=20.252 - 760.051 Torr; 0.5 - 4 h; Purification / work up;
参考文献
NIPPOH CHEMICALS CO., LTD.
Patent: WO2007/26766 A1, 2007 ;
Location in patent: Page/Page column 12; 13 ;
