2-巯基-4,6-二甲基嘧啶水合物合成路线 （共 27 条）
反应条件
poly(4-vinylpyridinium nitrate) I; silica supported sulfuric acid in ethyl acetate T=20°C; 1.75 h;
参考文献
Ghorbani-Choghamarani, Arash; Nikoorazm, Mohsen; Goudarziafshar, Hamid; Abbasi, Mina
Bulletin of the Korean Chemical Society, 2011 , vol. 32, # 2 p. 693 - 696
反应条件
1: 2-mercapto-4,6-dimethyl-pyrimidine With sulfuryl dichloride; triethylamine in dichloromethane T=0 - 20°C; 2: pyrrolidin-1-yl-2,5-dione With triethylamine in dichloromethane T=0 - 20°C; 1 h;
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851
反应条件
1: 60 percent / aq. KOH 2: 60 percent / hydrazine hydrate / ethanol / 6 h / Heating View Scheme
参考文献
Ouf
Bollettino chimico farmaceutico, 2004 , vol. 143, # 7 p. 275 - 279
反应条件
sodium hydroxide 1 h; Ambient temperature;
参考文献
Chemistry of Heterocyclic Compounds (New York, NY, United States), , vol. 28, # 5 p. 591 - 595
Khimiya Geterotsiklicheskikh Soedinenii, Sbornik, , # 5 p. 698 - 703
反应条件
in dichloromethane stirring (N2 atmosphere, room temp., 30min); concn. (vac.), dissoln. in CH2Cl2, TLC (SiO2, hexane/CH2Cl2=90/10);
参考文献
Inorganica Chimica Acta, , vol. 228, p. 267 - 275
反应条件
sodium hydroxide in ethanol; water
4 h; Ambient temperature;
参考文献
Schickaneder, Helmut; Engler, Heidrun; Szelenyi, Istvan
Journal of Medicinal Chemistry, 1987 , vol. 30, # 3 p. 547 - 551
反应条件
in 1,4-dioxane
T=20°C;
参考文献
Lanier, Marion; Sergienko, Eduard; Simao, Ana Maria; Su, Ying; Chung, Thomas; Millan, Jose Luis; Cashman, John R.
Bioorganic and Medicinal Chemistry, 2010 , vol. 18, # 2 p. 573 - 579
