反应条件
in xylene
refluxed, solvent removed, residue dissolved in CHCl3, stirring overnight; solvent removed, chromd. on alumina, elution with CH2Cl2-light petroleum (1:1), recrystn. from CH2Cl2-light petroleum, elem. anal.;
参考文献
Howell, James A. S.; Rowan, Anthony J.; Snell, Mark S.
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1981 , p. 325 - 327