(9CI)-吡咯并[1,2-c]嘧啶-1(2H)-酮合成路线 （共 3 条）
反应条件
1: 83 percent / NaBH4 / methanol / 0.33 h / 0 °C 2: 1.) Et3N, MeSO2Cl, 2.) NaOH / 1.) CH2Cl2, 0 deg C, 20 min, 2.) MeOH, 5 min View Scheme
参考文献
Alvarez, Mercedes; Fernandez, David; Joule, John A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 3 p. 249 - 255
反应条件
sodium hydroxide; methanesulfonyl chloride; triethylamine 1.) CH2Cl2, 0 deg C, 20 min, 2.) MeOH, 5 min; Yield given. Multistep reaction;
参考文献
Alvarez, Mercedes; Fernandez, David; Joule, John A.
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 3 p. 249 - 255
反应条件
sodium hydride in tetrahydrofuran 15 h; Ambient temperature;
参考文献
Alvarez, Mercedes; Fernandez, David; Joule, John A.
Journal of the Chemical Society. Perkin Transactions 1, 2002 , # 4 p. 471 - 475
