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63148-62-9
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471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
22346-57-2
合成路线
（共 10 条）
141861-64-5
→
反应条件
22346-57-2
反应条件
boron tribromide in dichloromethane 24 h; Ambient temperature;
参考文献
Elix, John A.; Crook, Caroline E.; Jiang, Hui; Zhi-ning, Zhu
Australian Journal of Chemistry, 1992 , vol. 45, # 5 p. 845 - 855
67065-98-9
→
反应条件
22346-57-2
+
67065-99-0
反应条件
N-chloro-succinimide; toluene-4-sulfonic acid in 1,4-dioxane 20 h; Heating;
参考文献
Elix, John A.; Jiang, Hui; Wardlaw, Judith H.
Australian Journal of Chemistry, 1990 , vol. 43, # 10 p. 1745 - 1758
57074-24-5
→
反应条件
22346-57-2
反应条件
1: 6 percent / diphenyl ether / 5 h / Heating 2: 65 percent / BBr3 / CH2Cl2 / 24 h / Ambient temperature View Scheme
参考文献
Elix, John A.; Crook, Caroline E.; Jiang, Hui; Zhi-ning, Zhu
Australian Journal of Chemistry, 1992 , vol. 45, # 5 p. 845 - 855
6110-36-7
2-羟基-4-甲氧基-6-甲基苯甲酸乙酯
→
反应条件
22346-57-2
反应条件
1: 90 percent / SO2Cl2 / diethyl ether / 17 h / Ambient temperature 2: 6 percent / diphenyl ether / 5 h / Heating 3: 65 percent / BBr3 / CH2Cl2 / 24 h / Ambient temperature View Scheme
参考文献
Elix, John A.; Crook, Caroline E.; Jiang, Hui; Zhi-ning, Zhu
Australian Journal of Chemistry, 1992 , vol. 45, # 5 p. 845 - 855
131524-54-4
→
反应条件
22346-57-2
反应条件
1: 76 percent / KOH / dimethylsulfoxide; H2O / 5 h / 100 - 110 °C 2: 11 percent / N-chlorosuccinimide, toluene-4-sulfonic acid / dioxane / 20 h / Heating View Scheme
参考文献
Elix, John A.; Jiang, Hui; Wardlaw, Judith H.
Australian Journal of Chemistry, 1990 , vol. 43, # 10 p. 1745 - 1758
131524-53-3
→
反应条件
22346-57-2
反应条件
1: 81 percent / boron trichloride / CH2Cl2 / 2 h / Ambient temperature 2: 11 percent / N-chlorosuccinimide, toluene-4-sulfonic acid / dioxane / 20 h / Heating View Scheme
参考文献
Elix, John A.; Jiang, Hui; Wardlaw, Judith H.
Australian Journal of Chemistry, 1990 , vol. 43, # 10 p. 1745 - 1758
131524-51-1
→
反应条件
22346-57-2
反应条件
1: 45 percent / KOH / dimethylsulfoxide; H2O / 5 h / 100 - 110 °C 2: 81 percent / boron trichloride / CH2Cl2 / 2 h / Ambient temperature 3: 11 percent / N-chlorosuccinimide, toluene-4-sulfonic acid / dioxane / 20 h / Heating View Scheme
参考文献
Elix, John A.; Jiang, Hui; Wardlaw, Judith H.
Australian Journal of Chemistry, 1990 , vol. 43, # 10 p. 1745 - 1758
131524-49-7
→
反应条件
22346-57-2
反应条件
1: 59 percent / trifluoroacetic anhydride / toluene / 1.) 0 deg C, 10 min, 2.) RT, 22 h 2: 45 percent / KOH / dimethylsulfoxide; H2O / 5 h / 100 - 110 °C 3: 81 percent / boron trichloride / CH2Cl2 / 2 h / Ambient temperature 4: 11 percent / N-chlorosuccinimide, toluene-4-sulfonic acid / dioxane / 20 h / Heating View Scheme
参考文献
Elix, John A.; Jiang, Hui; Wardlaw, Judith H.
Australian Journal of Chemistry, 1990 , vol. 43, # 10 p. 1745 - 1758
131524-52-2
→
反应条件
22346-57-2
反应条件
1: 93 percent / boron trichloride / CH2Cl2 / 3 h / Ambient temperature 2: 76 percent / KOH / dimethylsulfoxide; H2O / 5 h / 100 - 110 °C 3: 11 percent / N-chlorosuccinimide, toluene-4-sulfonic acid / dioxane / 20 h / Heating View Scheme
参考文献
Elix, John A.; Jiang, Hui; Wardlaw, Judith H.
Australian Journal of Chemistry, 1990 , vol. 43, # 10 p. 1745 - 1758
131524-50-0
→
反应条件
22346-57-2
反应条件
1: 87 percent / trifluoroacetic anhydride / toluene / 1.) 0 deg C, 10 min, 2.) RT, 22 h 2: 93 percent / boron trichloride / CH2Cl2 / 3 h / Ambient temperature 3: 76 percent / KOH / dimethylsulfoxide; H2O / 5 h / 100 - 110 °C 4: 11 percent / N-chlorosuccinimide, toluene-4-sulfonic acid / dioxane / 20 h / Heating View Scheme
参考文献
Elix, John A.; Jiang, Hui; Wardlaw, Judith H.
Australian Journal of Chemistry, 1990 , vol. 43, # 10 p. 1745 - 1758
