3-三氟甲基联苯-2-甲醛合成路线 (共 3 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); tripotassium phosphate monohydrate in ethylene glycol dimethyl ether T=150°C; Suzuki-Miyaura cross coupling; P=4500.45 Torr; 1.5 h; Microwave irradiation;
参考文献
Chosson, Elizabeth; Rochais, Christophe; Legay, Remi; Santos, Jana Sopkova De Oliveira; Rault, Sylvain; Dallemagne, Patrick
Tetrahedron, 2011 , vol. 67, # 14 p. 2548 - 2554
反应条件
bicyclo-[2.2.1]hept-2-ene; palladium diacetate; CsO2CCMe3 in N,N-dimethyl-formamide T=105°C; 24 h; Inert atmosphere;
参考文献
Motti, Elena; Ca, Nicola Della; Xu, Di; Piersimoni, Anna; Bedogni, Elena; Zhou, Zhi-Ming; Catellani, Marta
Organic Letters, 2012 , vol. 14, # 22 p. 5792 - 5795
反应条件
bicyclo-[2.2.1]hept-2-ene; palladium diacetate; potassium carbonate in N,N-dimethyl-formamide T=105°C; 24 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 14, # 22 p. 5792 - 5795