反应条件
1: 93 percent / LiAlH4, AlCl3 / diethyl ether / 1 h / Heating 2: 88 percent / pyridine / 0 - 20 °C 3: 99 percent / poly(phosphoric acid) / 4 h / 160 - 165 °C 4: 94 percent / phenyl disulfide / 1,2,3,4-tetrahydro-naphthalene / 15 h / 200 - 205 °C 5: 86 percent / 30percent aq. H2O2, glacial AcOH / 30 h / 65 - 70 °C 6: 1.) AcOH, AcONa, 2.) 10percent aq. HCl / 1.) from 80 deg C to 85 deg C, 2 h, 2.) reflux, 1 h 7: 86 percent / pyridine / 0 - 20 °C 8: 49 percent / SeO2 / dioxane / 3 h / Heating 9: aq. HCl / ethanol / Heating View Scheme
参考文献
Liu, Mao-Chin; Lin, Tai-Shun; Penketh, Philip; Sartorelli, Alan C.
Journal of Medicinal Chemistry, 1995 , vol. 38, # 21 p. 4234 - 4243
