potassium carbonate in chlorobenzene RefluxInert atmosphere;
参考文献
Sun, Aiming; Moore, Terry W.; Gunther, Jillian R.; Kim, Mi-Sun; Rhoden, Eric; Du, Yuhong; Fu, Haian; Snyder, James P.; Katzenellenbogen, John A.
ChemMedChem, 2011 , vol. 6, # 4 p. 654 - 666
1: 94 percent / pyridine / CH2Cl2 / 20 °C
2: 100 percent / CH2Cl2 / 0.17 h / 20 °C
3: 90 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C
View Scheme
参考文献
Meade, Eric A.; Sznaidman, Marcos; Pollard, Gerald T.; Beauchamp, Lilia M.; Howard, James L.
European Journal of Medicinal Chemistry, 1998 , vol. 33, # 5 p. 363 - 374
