1-甲基-3-苯基丙胺合成路线 (共 111 条)
反应条件
1: With ammonium formate in methanol T=80°C; 0.166667 h; Inert atmosphere; 2: With formic acid; C29H32ClIrNO; triethylamine in methanol T=80°C;
参考文献
Talwar, Dinesh; Salguero, Noemi Poyatos; Robertson, Craig M.; Xiao, Jianliang
Chemistry - A European Journal, 2014 , vol. 20, # 1 p. 245 - 252
反应条件
tri-ruthenium(0)dodecacarbonyl; ammonia; N-phenyl-2-(dicyclohexylphosphino)pyrrol in 1,1-dimethylpropan-1-ol T=150°C; 20 h; Cooling with dry iceMolecular sieve; chemoselective reaction;
参考文献
Imm, Sebastian; Neubert, Lorenz; Neumann, Helfried; Beller, Matthias
Angewandte Chemie - International Edition, 2010 , vol. 49, # 44 p. 8126 - 8129
反应条件
1: With 4-toluenesulfonyl azide; [N-3,5-di-t-Bu-salicylidene-2,2-diphenyl-glycinato]-Co(III); tetramethyldisiloxane in decane; ethanol T=23°C; 4 h; 2: With sodium tetrahydroborate; copper(II) sulfate in methanol T=0 - 23°C;
参考文献
Waser, Jerome; Nambu, Hisanori; Carreira, Erick M.
Journal of the American Chemical Society, 2005 , vol. 127, # 23 p. 8294 - 8295
反应条件
2,2,2-trifluoroethyl mercaptan in toluene T=22 - 24°C; Photolysis;
参考文献
El Blidi, Lahssen; Nechab, Malek; Vanthuyne, Nicolas; Gastaldi, Stephane; Bertrand, Michele P.; Gil, Gerard
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2901 - 2903
反应条件
perchloric acid; sodium perchlorate in water; acetonitrile T=0°C; Electrochemical reaction;
参考文献
De Marin, Sandra Lamo; Martens, Thierry; Mioskowski, Charles; Royer, Jacques
Journal of Organic Chemistry, 2005 , vol. 70, # 25 p. 10592 - 10595
反应条件
sodium tetrahydroborate; nickel dichloride in methanol T=-30°C;
参考文献
Ipaktschi, Junes
Chemische Berichte, 1984 , vol. 117, # 2 p. 856 - 858
反应条件
hydrogen; palladium on activated charcoal in ethanol
参考文献
Merli; Melloni; Tamagnone; Mascellani; Andriuoli; Micheli; Sarret; Brufani
Farmaco, Edizione Scientifica, 1982 , vol. 37, # 12 p. 824 - 835
反应条件
1: With oxygen in toluene T=100°C; 24 h; 2: With hydrogenchloride in methanol; water; toluene 12 h; 3: With sodium hydroxide in water pH=12 - 13;
参考文献
Miyamura, Hiroyuki; Morita, Masataka; Inasaki, Takeshi; Kobayashi, Shu
Bulletin of the Chemical Society of Japan, 2011 , vol. 84, # 6 p. 588 - 599
反应条件
hydrogen; nickel in methanol 24 h;
参考文献
Batra, Sanjay; Seth, M; Bhaduri, A P
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1992 , vol. 31, # 1 p. 60 - 62
反应条件
2,2,2-trifluoroethyl mercaptan in tetrahydrofuran; 3-methyl pentan-3-ol T=22 - 24°C; 2 h; Photolysis;
参考文献
Journal of Organic Chemistry, , vol. 74, # 7 p. 2901 - 2903