1-甲基-3-苯基丙胺合成路线 (共 111 条)
反应条件
Candida antarctica lipase B in n-heptane T=80°C; 6 h;
参考文献
Nechab, Malek; Azzi, Nadia; Vanthuyne, Nicolas; Bertrand, Michele; Gastaldi, Stephane; Gil, Gerard
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 6918 - 6923
反应条件
Candida antarctica lipase B in n-heptane T=80°C; 6 h;
参考文献
Nechab, Malek; Azzi, Nadia; Vanthuyne, Nicolas; Bertrand, Michele; Gastaldi, Stephane; Gil, Gerard
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 6918 - 6923
反应条件
Candida antarctica lipase B in n-heptane T=80°C; 5 h;
参考文献
Nechab, Malek; Azzi, Nadia; Vanthuyne, Nicolas; Bertrand, Michele; Gastaldi, Stephane; Gil, Gerard
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 6918 - 6923
反应条件
immobilized alkaline protease in 3-methyl pentan-3-ol T=21°C; 1 h; Enzymatic reaction; optical yield given as percent eediastereoselective reaction;
参考文献
El Blidi, Lahssen; Vanthuyne, Nicolas; Siri, Didier; Gastaldi, Stephane; Bertrand, Michele P.; Gil, Gerard
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 18 p. 4165 - 4168
反应条件
Candida antarctica lipase B in n-heptane T=80°C; 1.5 h;
参考文献
Nechab, Malek; Azzi, Nadia; Vanthuyne, Nicolas; Bertrand, Michele; Gastaldi, Stephane; Gil, Gerard
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 6918 - 6923
反应条件
Candida antarctica lipase B in n-heptane T=80°C; 9 h;
参考文献
Nechab, Malek; Azzi, Nadia; Vanthuyne, Nicolas; Bertrand, Michele; Gastaldi, Stephane; Gil, Gerard
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 6918 - 6923
反应条件
Candida antarctica lipase B in n-heptane T=80°C; 7 h;
参考文献
Nechab, Malek; Azzi, Nadia; Vanthuyne, Nicolas; Bertrand, Michele; Gastaldi, Stephane; Gil, Gerard
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 6918 - 6923
反应条件
alkaline protease in tetrahydrofuran; 3-methyl pentan-3-ol T=18 - 24°C; Enzymatic reaction; optical yield given as percent ee;
参考文献
El Blidi, Lahssen; Nechab, Malek; Vanthuyne, Nicolas; Gastaldi, Stephane; Bertrand, Michele P.; Gil, Gerard
Journal of Organic Chemistry, 2009 , vol. 74, # 7 p. 2901 - 2903
反应条件
Candida antarctica lipase B in n-heptane T=80°C; 5 h;
参考文献
Nechab, Malek; Azzi, Nadia; Vanthuyne, Nicolas; Bertrand, Michele; Gastaldi, Stephane; Gil, Gerard
Journal of Organic Chemistry, 2007 , vol. 72, # 18 p. 6918 - 6923
反应条件
immobilized Properase 1600L in 3-methyl pentan-3-ol T=21°C; 0.75 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Queyroy, Severine; Vanthuyne, Nicolas; Gastaldi, Stephane; Bertrand, Michele P.; Gil, Gerard
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 9 p. 1759 - 1764